2-(2',3',4',6'-tetra-O-benzyl-β-D-glucopyranosyl)-1-trifluoromethanesulfonyloxy-3,4,5-trimethoxybenzene

Base Information

Chemical Name:2-(2',3',4',6'-tetra-O-benzyl-β-D-glucopyranosyl)-1-trifluoromethanesulfonyloxy-3,4,5-trimethoxybenzene
CAS No.:458569-20-5
Molecular Formula:C₄₄H₄₅F₃O₁₁S
Molecular Weight:838.896
Hs Code.:

Synonyms:2-(2',3',4',6'-tetra-O-benzyl-β-D-glucopyranosyl)-1-trifluoromethanesulfonyloxy-3,4,5-trimethoxybenzene

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Chemical Property of 2-(2',3',4',6'-tetra-O-benzyl-β-D-glucopyranosyl)-1-trifluoromethanesulfonyloxy-3,4,5-trimethoxybenzene

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Technology Process of 2-(2',3',4',6'-tetra-O-benzyl-β-D-glucopyranosyl)-1-trifluoromethanesulfonyloxy-3,4,5-trimethoxybenzene

There total 4 articles about 2-(2',3',4',6'-tetra-O-benzyl-β-D-glucopyranosyl)-1-trifluoromethanesulfonyloxy-3,4,5-trimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 350480-15-8
2-(2',3',4',6'-tetra-O-benzyl-β-D-glucopyranosyl)-3,4,5-trimethoxyphen-1-ol

: 458569-20-5
2-(2',3',4',6'-tetra-O-benzyl-β-D-glucopyranosyl)-1-trifluoromethanesulfonyloxy-3,4,5-trimethoxybenzene

Guidance literature:: With dmap; lutidine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/ol026378e

Reference yield:

: 642-71-7
3,4,5-trimethoxyphenol

: 458569-20-5
2-(2',3',4',6'-tetra-O-benzyl-β-D-glucopyranosyl)-1-trifluoromethanesulfonyloxy-3,4,5-trimethoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / trimethylsilyl trifluoromethanesulfonate / CH₂Cl₂; toluene / -30 - 20 °C

2: 82 percent / lutidine; DMAP / CH₂Cl₂ / 0 - 20 °C

With dmap; trimethylsilyl trifluoromethanesulfonate; lutidine; In dichloromethane; toluene;
DOI:10.1021/ol026378e

Reference yield:

: 132201-75-3
2,3,4,6-tetra-O-benzyl-D-glucopyranose trichloroacetimidate

: 458569-20-5
2-(2',3',4',6'-tetra-O-benzyl-β-D-glucopyranosyl)-1-trifluoromethanesulfonyloxy-3,4,5-trimethoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / trimethylsilyl trifluoromethanesulfonate / CH₂Cl₂; toluene / -30 - 20 °C

2: 82 percent / lutidine; DMAP / CH₂Cl₂ / 0 - 20 °C

With dmap; trimethylsilyl trifluoromethanesulfonate; lutidine; In dichloromethane; toluene;
DOI:10.1021/ol026378e