1,4-diphenyl-1,4-diarsa-2,3,5-trithiacyclopentane

Base Information

• Chemical Name: 1,4-diphenyl-1,4-diarsa-2,3,5-trithiacyclopentane
• CAS No.: 35852-29-0
• Molecular Formula: C₁₂H₁₀As₂S₃
• Molecular Weight: 400.253
• Mol file: 35852-29-0.mol

Synonyms:1,4-diphenyl-1,4-diarsa-2,3,5-trithiacyclopentane

Chemical Property of 1,4-diphenyl-1,4-diarsa-2,3,5-trithiacyclopentane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,4-diphenyl-1,4-diarsa-2,3,5-trithiacyclopentane

There total 4 articles about 1,4-diphenyl-1,4-diarsa-2,3,5-trithiacyclopentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

phenylarsonic acid (98-05-5) → 1,4-diphenyl-1,4-diarsa-2,3,5-trithiacyclopentane (35852-29-0)

Guidance literature:

With hydrogen sulfide; In water; for 1.5h; cooling;

DOI:10.1039/b610228j

Reference yield:

phenyl-α-carboxyethylarsinic acid → 1,4-diphenyl-1,4-diarsa-2,3,5-trithiacyclopentane (35852-29-0)

Guidance literature:

With hydrogen sulfide; In ethanol; Yield given; Ambient temperature;

Reference yield:

dichlorophenylarsine (696-28-6) → 1,4-diphenyl-1,4-diarsa-2,3,5-trithiacyclopentane (35852-29-0)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydroxide / H₂O / 3 h / Ambient temperature

2: H₂S / ethanol / Ambient temperature

With sodium hydroxide; hydrogen sulfide; In ethanol; water;

upstream raw materials:

phenylarsonic acid

phenylcarboxymethylarsinic acid

dichlorophenylarsine

Downstream raw materials:

[Cu₄(C₆H₅(S)AsAs(S)C₆H₅)2(P(C₂H₅)3)4]