2-benzyloxy-5,6,12,12a-tetrahydro-3,9,10-trimethoxydibenz[b,g]indolizine

Base Information

• Chemical Name: 2-benzyloxy-5,6,12,12a-tetrahydro-3,9,10-trimethoxydibenz[b,g]indolizine
• CAS No.: 17138-39-5
• Molecular Formula: C₂₆H₂₇NO₄
• Molecular Weight: 417.505

Synonyms:2-benzyloxy-5,6,12,12a-tetrahydro-3,9,10-trimethoxydibenz[b,g]indolizine

Chemical Property of 2-benzyloxy-5,6,12,12a-tetrahydro-3,9,10-trimethoxydibenz[b,g]indolizine

Chemical Property:

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Technology Process of 2-benzyloxy-5,6,12,12a-tetrahydro-3,9,10-trimethoxydibenz[b,g]indolizine

There total 22 articles about 2-benzyloxy-5,6,12,12a-tetrahydro-3,9,10-trimethoxydibenz[b,g]indolizine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

7-benzyloxy-1-(2-bromo-4,5-dimethoxybenzyl)-1,2,3,4-tetrahydro-6-methoxyisoquinoline (47706-26-3) → 2-benzyloxy-5,6,12,12a-tetrahydro-3,9,10-trimethoxydibenz[b,g]indolizine (17138-39-5)

Guidance literature:

With sodium t-butanolate; (IMes)2Pd(η3-allyl)Cl; In toluene; at 80 ℃; for 14h;

DOI:10.1055/s-2003-41468

Reference yield: 90.0%

2-benzyloxy-3,9,10-trimethoxy-5,6-dihydroindolo[2,1-a]isoquinoline → 2-benzyloxy-5,6,12,12a-tetrahydro-3,9,10-trimethoxydibenz[b,g]indolizine (17138-39-5)

Guidance literature:

With sodium cyanoborohydride; In acetic acid;

DOI:10.1021/ol005802d

Reference yield: 60.0%

7-Benzyloxy-2-(4,5-dimethoxy-2-trimethylsilanylmethyl-phenyl)-6-methoxy-3,4-dihydro-isoquinolinium; chloride → 2-benzyloxy-5,6,12,12a-tetrahydro-3,9,10-trimethoxydibenz[b,g]indolizine (17138-39-5)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; Heating;

DOI:10.3987/R-1987-06-1483

upstream raw materials:

1-[2-(4-Benzyloxy-2-bromo-5-methoxy-phenyl)-ethyl]-5,6-dimethoxy-1H-indole

7-benzyloxy-1-(2-bromo-4,5-dimethoxybenzyl)-1,2,3,4-tetrahydro-6-methoxyisoquinoline

7-benzyloxy-1-(2-bromo-4,5-dimethoxy-benzyl)-6-methoxy-3,4-dihydro-isoquinoline

2-(4-(benzyloxy)-3-methoxyphenyl)acetyl chloride

Downstream raw materials:

2,2'-Bis-benzyloxy-3,9,10,3',9',10'-hexamethoxy-5,6,5',6'-tetrahydro-[12,12']bi[indolo[2,1-a]isoquinolinyl]

(+/-)-O-benzylcryptaustoline

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