benzyl 2-azido-4-O-benzoyl-3-O-benzyl-2-deoxy-α-D-xylopyranoside

Base Information

• Chemical Name: benzyl 2-azido-4-O-benzoyl-3-O-benzyl-2-deoxy-α-D-xylopyranoside
• CAS No.: 109200-30-8
• Molecular Formula: C₂₆H₂₅N₃O₅
• Molecular Weight: 459.502
• Mol file: 109200-30-8.mol

Synonyms:benzyl 2-azido-4-O-benzoyl-3-O-benzyl-2-deoxy-α-D-xylopyranoside

Chemical Property of benzyl 2-azido-4-O-benzoyl-3-O-benzyl-2-deoxy-α-D-xylopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of benzyl 2-azido-4-O-benzoyl-3-O-benzyl-2-deoxy-α-D-xylopyranoside

There total 5 articles about benzyl 2-azido-4-O-benzoyl-3-O-benzyl-2-deoxy-α-D-xylopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

benzyl bromide (100-39-0) + benzyl 2-azido-4-O-benzoyl-2-deoxy-α-D-xylopyranoside (109200-28-4) → benzyl 2-azido-4-O-benzoyl-3-O-benzyl-2-deoxy-α-D-xylopyranoside (109200-30-8)

Guidance literature:

With silver(l) oxide; In benzene; for 40h; exclusion of light;

DOI:10.1246/bcsj.59.3131

Reference yield:

benzyl 3,4-di-O-acetyl-2-azido-2-deoxy-α-D-xylopyranoside (109200-15-9) → benzyl 2-azido-4-O-benzoyl-3-O-benzyl-2-deoxy-α-D-xylopyranoside (109200-30-8)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium / methanol / Ambient temperature

2: 66 percent / triethylamine / acetone / 16 h / Ambient temperature

3: 86 percent / silver oxide / benzene / 40 h / exclusion of light

With sodium; triethylamine; silver(l) oxide; In methanol; acetone; benzene;

DOI:10.1246/bcsj.59.3131

Reference yield:

benzyl 2-azido-2-deoxy-α-D-xylopyranoside (109200-27-3) → benzyl 2-azido-4-O-benzoyl-3-O-benzyl-2-deoxy-α-D-xylopyranoside (109200-30-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 66 percent / triethylamine / acetone / 16 h / Ambient temperature

2: 86 percent / silver oxide / benzene / 40 h / exclusion of light

With triethylamine; silver(l) oxide; In acetone; benzene;

DOI:10.1246/bcsj.59.3131

upstream raw materials:

benzyl bromide

benzyl 2-azido-4-O-benzoyl-2-deoxy-α-D-xylopyranoside

benzyl 3,4-di-O-acetyl-2-azido-2-deoxy-α-D-xylopyranoside

benzyl 2-azido-2-deoxy-α-D-xylopyranoside

Downstream raw materials:

benzyl 2-azido-3-O-benzyl-2-deoxy-α-D-xylopyranoside