C₆₄H₈₀O₁₀

Base Information

• Chemical Name: C₆₄H₈₀O₁₀
• CAS No.: 1558035-00-9
• Molecular Formula: C₆₄H₈₀O₁₀
• Molecular Weight: 1009.33
• Mol file: 1558035-00-9.mol

Synonyms:C₆₄H₈₀O₁₀

Chemical Property of C₆₄H₈₀O₁₀

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₄H₈₀O₁₀

There total 9 articles about C₆₄H₈₀O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

C38H38O8 (1558034-99-3) + (3S,4R)-4-(4-methoxybenzyloxy)octadec-1-en-3-ol (1558034-96-0) → C64H80O10 (1558035-00-9)

Guidance literature:

C₃₈H₃₈O₈; With 2,4,6-trichlorobenzoyl chloride; triethylamine; In tetrahydrofuran; at 0 ℃; for 4h; Inert atmosphere;

(3S,4R)-4-(4-methoxybenzyloxy)octadec-1-en-3-ol; With dmap; In tetrahydrofuran; toluene; at 20 ℃; for 1h; Inert atmosphere;

DOI:10.1021/ol5002686

Reference yield:

phthalic anhydride (85-44-9) → C64H80O10 (1558035-00-9)

Guidance literature:

Multi-step reaction with 2 steps

1.1: pyridine; dmap / 16 h / 20 °C / Inert atmosphere

2.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / tetrahydrofuran / 4 h / 0 °C / Inert atmosphere

2.2: 1 h / 20 °C / Inert atmosphere

With pyridine; dmap; 2,4,6-trichlorobenzoyl chloride; triethylamine; In tetrahydrofuran;

DOI:10.1021/ol5002686

Reference yield:

1-(3',4',6'-tri-O-benzyl-α-D-galactopyranosyl)-2-propene (271246-08-3) → C64H80O10 (1558035-00-9)

Guidance literature:

Multi-step reaction with 2 steps

1.1: pyridine; dmap / 16 h / 20 °C / Inert atmosphere

2.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / tetrahydrofuran / 4 h / 0 °C / Inert atmosphere

2.2: 1 h / 20 °C / Inert atmosphere

With pyridine; dmap; 2,4,6-trichlorobenzoyl chloride; triethylamine; In tetrahydrofuran;

DOI:10.1021/ol5002686

upstream raw materials:

1-(3',4',6'-tri-O-benzyl-α-D-galactopyranosyl)-2-propene

C₃₈H₃₈O₈

(3S,4R)-4-(4-methoxybenzyloxy)octadec-1-en-3-ol

1-tetradecene

Downstream raw materials:

C₆₂H₇₆O₁₀

C₅₄H₇₄O₈

C₆₈H₈₆O₈

C₆₀H₇₈O₇