Technology Process of methyl 4-(1-methoxyethyl)-3-nitrobenzoate
There total 5 articles about methyl 4-(1-methoxyethyl)-3-nitrobenzoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: nitric acid; sulfuric acid / water / 3 h / 20 °C
2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 6 h / 20 °C
3: methanol / 0.5 h
4: N-Bromosuccinimide; Perbenzoic acid / benzene / 14 h / Reflux; Darkness
5: silver nitrate / 20 °C / Darkness
With
N-Bromosuccinimide; Perbenzoic acid; sulfuric acid; nitric acid; silver nitrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
methanol; dichloromethane; water; benzene;
DOI:10.1021/la500744s
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 6 h / 20 °C
2: methanol / 0.5 h
3: N-Bromosuccinimide; Perbenzoic acid / benzene / 14 h / Reflux; Darkness
4: silver nitrate / 20 °C / Darkness
With
N-Bromosuccinimide; Perbenzoic acid; silver nitrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
methanol; dichloromethane; benzene;
DOI:10.1021/la500744s
- Guidance literature:
-
Multi-step reaction with 3 steps
1: methanol / 0.5 h
2: N-Bromosuccinimide; Perbenzoic acid / benzene / 14 h / Reflux; Darkness
3: silver nitrate / 20 °C / Darkness
With
N-Bromosuccinimide; Perbenzoic acid; silver nitrate;
In
methanol; benzene;
DOI:10.1021/la500744s
