Technology Process of C43H45N10O12P
There total 9 articles about C43H45N10O12P which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 84 percent / pyridine / 1 h / 20 °C
2.1: diphenyl phosphonate / pyridine / 1.5 h / 20 °C
2.2: 77 percent / H2O / 1 h / 20 °C
3.1: 88 percent / BOP-Cl / pyridine / 1.5 h / 20 °C
With
diphenyl hydrogen phosphite; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride;
In
pyridine;
DOI:10.1016/S0040-4039(01)02028-7
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: TMSCl / acetonitrile / 1 h / 20 °C
2.1: ethanol / 1 h / 20 °C
3.1: 83 percent / Et3N; DMAP / CH2Cl2 / 48 h / 20 °C
4.1: TMSN3; BuONO / CH2Cl2 / 24 h / -20 - 20 °C
4.2: 45 percent / H2O; methanol / 1 h / 20 °C
5.1: 89 percent / conc. NH3 / dioxane / 60 h / 20 °C
6.1: 84 percent / pyridine / 1 h / 20 °C
7.1: diphenyl phosphonate / pyridine / 1.5 h / 20 °C
7.2: 77 percent / H2O / 1 h / 20 °C
8.1: 88 percent / BOP-Cl / pyridine / 1.5 h / 20 °C
With
dmap; ammonium hydroxide; chloro-trimethyl-silane; n-Butyl nitrite; trimethylsilylazide; diphenyl hydrogen phosphite; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine;
In
1,4-dioxane; pyridine; ethanol; dichloromethane; acetonitrile;
DOI:10.1016/S0040-4039(01)02028-7