N-Me-Ala-4-nitrobenzylamide hydrochloride

Base Information

Chemical Name:N-Me-Ala-4-nitrobenzylamide hydrochloride
CAS No.:928211-71-6
Molecular Formula:C₁₁H₁₅N₃O₃*ClH
Molecular Weight:273.719
Hs Code.:

Synonyms:N-Me-Ala-4-nitrobenzylamide hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-Me-Ala-4-nitrobenzylamide hydrochloride

Chemical Property:

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Technology Process of N-Me-Ala-4-nitrobenzylamide hydrochloride

There total 1 articles about N-Me-Ala-4-nitrobenzylamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 928211-70-5
Boc-N-Me-Ala-4-nitrobenzylamide

: 928211-71-6
N-Me-Ala-4-nitrobenzylamide hydrochloride

Guidance literature:: With hydrogenchloride; In ethyl acetate; at -78 ℃;

Reference yield:

: 928211-73-8
(4-chlorobenzylsulfonyl)-D-Ser(O-tBu)-Cl

: 928211-71-6
N-Me-Ala-4-nitrobenzylamide hydrochloride

: 928211-75-0
(4-chlorobenzylsulfonyl)-D-Ser(O-tBu)-N-Me-Ala-4-nitro-benzylamide

Guidance literature:: N-Me-Ala-4-nitrobenzylamide hydrochloride; With N-ethyl-N,N-diisopropylamine; In dichloromethane;

(4-chlorobenzylsulfonyl)-D-Ser(O-tBu)-Cl; In dichloromethane; at 20 ℃; Cooling with ice;

Reference yield:

: 928211-71-6
N-Me-Ala-4-nitrobenzylamide hydrochloride

: 928211-79-4
(4-chlorobenzylsulfonyl)-D-Ser-N-Me-Ala-4-(N-cyan-amino)benzylamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane

1.2: 20 °C / Cooling with ice

2.1: methyl-phenyl-thioether; trifluoroacetic acid / 20 °C

3.1: hydrogen / palladium 10% on activated carbon / methanol

3.2: 1.5 h / 0 °C

4.1: sodium acetate / ethanol / 20 °C

With methyl-phenyl-thioether; hydrogen; sodium acetate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; palladium 10% on activated carbon; In methanol; ethanol; dichloromethane;