WX-582

Base Information

Chemical Name:WX-582
CAS No.:552288-37-6
Molecular Formula:C₂₂H₂₉ClN₆O₅S
Molecular Weight:525.028
Hs Code.:

Synonyms:

Suppliers and Price of WX-582

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of WX-582

Chemical Property:

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Technology Process of WX-582

There total 11 articles about WX-582 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 928211-73-8
(4-chlorobenzylsulfonyl)-D-Ser(O-tBu)-Cl

: 552288-37-6
WX-582

Guidance literature:: Multi-step reaction with 7 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane

1.2: 20 °C / Cooling with ice

2.1: methyl-phenyl-thioether; trifluoroacetic acid / 20 °C

3.1: hydrogen / palladium 10% on activated carbon / methanol

3.2: 1.5 h / 0 °C

4.1: sodium acetate / ethanol / 20 °C

5.1: hydroxylamine hydrochloride; N-ethyl-N,N-diisopropylamine / ethanol / 20 °C / Cooling with ice

6.1: 1-methyl-pyrrolidin-2-one / 20 °C

7.1: liver homogenate / 2 h / Enzymatic reaction

With methyl-phenyl-thioether; hydroxylamine hydrochloride; hydrogen; sodium acetate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; palladium 10% on activated carbon; In 1-methyl-pyrrolidin-2-one; methanol; ethanol; dichloromethane;

Reference yield:

: 928211-71-6
N-Me-Ala-4-nitrobenzylamide hydrochloride

: 552288-37-6
WX-582

Guidance literature:: Multi-step reaction with 7 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane

1.2: 20 °C / Cooling with ice

2.1: methyl-phenyl-thioether; trifluoroacetic acid / 20 °C

3.1: hydrogen / palladium 10% on activated carbon / methanol

3.2: 1.5 h / 0 °C

4.1: sodium acetate / ethanol / 20 °C

5.1: hydroxylamine hydrochloride; N-ethyl-N,N-diisopropylamine / ethanol / 20 °C / Cooling with ice

6.1: 1-methyl-pyrrolidin-2-one / 20 °C

7.1: liver homogenate / 2 h / Enzymatic reaction

With methyl-phenyl-thioether; hydroxylamine hydrochloride; hydrogen; sodium acetate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; palladium 10% on activated carbon; In 1-methyl-pyrrolidin-2-one; methanol; ethanol; dichloromethane;

Reference yield:

: 928211-75-0
(4-chlorobenzylsulfonyl)-D-Ser(O-tBu)-N-Me-Ala-4-nitro-benzylamide

: 552288-37-6
WX-582

Guidance literature:: Multi-step reaction with 6 steps

1.1: methyl-phenyl-thioether; trifluoroacetic acid / 20 °C

2.1: hydrogen / palladium 10% on activated carbon / methanol

2.2: 1.5 h / 0 °C

3.1: sodium acetate / ethanol / 20 °C

4.1: hydroxylamine hydrochloride; N-ethyl-N,N-diisopropylamine / ethanol / 20 °C / Cooling with ice

5.1: 1-methyl-pyrrolidin-2-one / 20 °C

6.1: liver homogenate / 2 h / Enzymatic reaction

With methyl-phenyl-thioether; hydroxylamine hydrochloride; hydrogen; sodium acetate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; palladium 10% on activated carbon; In 1-methyl-pyrrolidin-2-one; methanol; ethanol;