C₃₂H₁₆F₅NO₂

Base Information

• Chemical Name: C₃₂H₁₆F₅NO₂
• CAS No.: 1309688-77-4
• Molecular Formula: C₃₂H₁₆F₅NO₂
• Molecular Weight: 541.477
• Mol file: 1309688-77-4.mol

Synonyms:C₃₂H₁₆F₅NO₂

Chemical Property of C₃₂H₁₆F₅NO₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₂H₁₆F₅NO₂

There total 4 articles about C₃₂H₁₆F₅NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C18H11F3O4S → C32H16F5NO2 (1309688-77-4)

Guidance literature:

Multi-step reaction with 3 steps

1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutylammomium bromide; triethylamine / N,N-dimethyl-formamide / Heating

2: pyridine; hydroxylamine hydrochloride / Heating

3: triethylamine / dichloromethane / Cooling

With pyridine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; hydroxylamine hydrochloride; tetrabutylammomium bromide; triethylamine; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1055/s-0030-1259556

Reference yield:

C25H16O → C32H16F5NO2 (1309688-77-4)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine; hydroxylamine hydrochloride / Heating

2: triethylamine / dichloromethane / Cooling

With pyridine; hydroxylamine hydrochloride; triethylamine; In dichloromethane;

DOI:10.1055/s-0030-1259556

Reference yield:

(2-hydroxyphenyl)(naphthalen-2-yl)methanone (93327-64-1) → C32H16F5NO2 (1309688-77-4)

Guidance literature:

Multi-step reaction with 4 steps

1: pyridine; dmap / dichloromethane / Cooling

2: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutylammomium bromide; triethylamine / N,N-dimethyl-formamide / Heating

3: pyridine; hydroxylamine hydrochloride / Heating

4: triethylamine / dichloromethane / Cooling

With pyridine; dmap; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; hydroxylamine hydrochloride; tetrabutylammomium bromide; triethylamine; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1055/s-0030-1259556

upstream raw materials:

pentafluorobenzoylchloride

(2-hydroxyphenyl)(naphthalen-2-yl)methanone

Downstream raw materials:

C₂₅H₁₇N