trans-chlorobis(triphenylphosphine)(C₈H₈N₂)palladium tetrafluoroborate

Base Information

• Chemical Name: trans-chlorobis(triphenylphosphine)(C₈H₈N₂)palladium tetrafluoroborate
• CAS No.: 676491-73-9
• Molecular Formula: BF₄*C₄₄H₃₈ClN₂P₂Pd
• Molecular Weight: 885.424

Synonyms:trans-chlorobis(triphenylphosphine)(C₈H₈N₂)palladium tetrafluoroborate

Chemical Property of trans-chlorobis(triphenylphosphine)(C₈H₈N₂)palladium tetrafluoroborate

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Technology Process of trans-chlorobis(triphenylphosphine)(C₈H₈N₂)palladium tetrafluoroborate

There total 1 articles about trans-chlorobis(triphenylphosphine)(C₈H₈N₂)palladium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.9%

trans-chlorobis(triphenylphosphine)(2-(azidomethyl)phenylisocyanido)palladium tetrafluoroborate (676491-68-2) → trans-chlorobis(triphenylphosphine)(C8H8N2)palladium tetrafluoroborate (676491-73-9)

Guidance literature:

With triphenyl phosphine; In dichloromethane; byproducts: N2, triphenyl phosphinoxide; under N2; PPh3 added to soln. of Pd-complex, stirred at room temp. for 12 h; Et2O added, ppt. filtered off, washed with Et2O, dried in vacuo; elem. anal.;

DOI:10.1016/j.jorganchem.2003.10.029

upstream raw materials:

trans-chlorobis(triphenylphosphine)(2-(azidomethyl)phenylisocyanido)palladium tetrafluoroborate

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