trans-chlorobis(triphenylphosphine)(2-(azidomethyl)phenylisocyanido)palladium tetrafluoroborate

Base Information

Chemical Name:trans-chlorobis(triphenylphosphine)(2-(azidomethyl)phenylisocyanido)palladium tetrafluoroborate
CAS No.:676491-68-2
Molecular Formula:BF₄*C₄₄H₃₆ClN₄P₂Pd
Molecular Weight:911.422
Hs Code.:

Synonyms:trans-chlorobis(triphenylphosphine)(2-(azidomethyl)phenylisocyanido)palladium tetrafluoroborate

Suppliers and Price of trans-chlorobis(triphenylphosphine)(2-(azidomethyl)phenylisocyanido)palladium tetrafluoroborate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of trans-chlorobis(triphenylphosphine)(2-(azidomethyl)phenylisocyanido)palladium tetrafluoroborate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of trans-chlorobis(triphenylphosphine)(2-(azidomethyl)phenylisocyanido)palladium tetrafluoroborate

There total 1 articles about trans-chlorobis(triphenylphosphine)(2-(azidomethyl)phenylisocyanido)palladium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.3%

: 13965-03-2
bis-triphenylphosphine-palladium(II) chloride

: 14104-20-2
silver tetrafluoroborate

: 496963-67-8
1-(azidomethyl)-2-isocyanobenzene

: 676491-68-2
trans-chlorobis(triphenylphosphine)(2-(azidomethyl)phenylisocyanido)palladium tetrafluoroborate

Guidance literature:: In dichloromethane; acetone; byproducts: AgCl; under N2; 1 M soln. of AgBF4 in acetone added to a suspn. of Pd-complex in CH2Cl2 at room temp., stirred for 30 min., AgCl filtered off, filtrate treated with isonitrile, stirred for 2.5 h; Et2O added, ppt. filtered off, dried under vac.; elem. anal.;
DOI:10.1016/j.jorganchem.2003.10.029

Reference yield: 87.9%

: 676491-68-2
trans-chlorobis(triphenylphosphine)(2-(azidomethyl)phenylisocyanido)palladium tetrafluoroborate

: 676491-73-9
trans-chlorobis(triphenylphosphine)(C₈H₈N₂)palladium tetrafluoroborate

Guidance literature:: With triphenyl phosphine; In dichloromethane; byproducts: N2, triphenyl phosphinoxide; under N2; PPh3 added to soln. of Pd-complex, stirred at room temp. for 12 h; Et2O added, ppt. filtered off, washed with Et2O, dried in vacuo; elem. anal.;
DOI:10.1016/j.jorganchem.2003.10.029