1-((6Z,10Z)-12-Benzyloxy-2,6,10-trimethyl-dodeca-2,6,10-triene-4-sulfonyl)-4-methyl-benzene

Base Information

Chemical Name:1-((6Z,10Z)-12-Benzyloxy-2,6,10-trimethyl-dodeca-2,6,10-triene-4-sulfonyl)-4-methyl-benzene
CAS No.:86636-50-2
Molecular Formula:C₂₉H₃₈O₃S
Molecular Weight:466.685
Hs Code.:

Synonyms:1-((6Z,10Z)-12-Benzyloxy-2,6,10-trimethyl-dodeca-2,6,10-triene-4-sulfonyl)-4-methyl-benzene

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Chemical Property of 1-((6Z,10Z)-12-Benzyloxy-2,6,10-trimethyl-dodeca-2,6,10-triene-4-sulfonyl)-4-methyl-benzene

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Technology Process of 1-((6Z,10Z)-12-Benzyloxy-2,6,10-trimethyl-dodeca-2,6,10-triene-4-sulfonyl)-4-methyl-benzene

There total 3 articles about 1-((6Z,10Z)-12-Benzyloxy-2,6,10-trimethyl-dodeca-2,6,10-triene-4-sulfonyl)-4-methyl-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 86636-47-7
(2Z,6Z)-8-(benzyloxy)-2,6-dimethyl-1-(tetrahydropyran-2-yloxy)-octa-2,6-diene

: 86636-50-2
1-((6Z,10Z)-12-Benzyloxy-2,6,10-trimethyl-dodeca-2,6,10-triene-4-sulfonyl)-4-methyl-benzene

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / p-TsOH / methanol / 27 h / Ambient temperature

3: 1.) n-BuLi, THF, HMPA, -40 to -30 deg C; 2.) -60 to 0 deg C / different sulphones investigated

With tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; toluene-4-sulfonic acid; In methanol;
DOI:10.1246/cl.1983.725

Reference yield:

: 52188-74-6,70238-38-9,94854-66-7,115425-27-9,130487-40-0,86636-48-8
(2Z,6Z)-8-(benzyloxy)-2,6-dimethylocta-2,6-dien-1-ol

: 86636-50-2
1-((6Z,10Z)-12-Benzyloxy-2,6,10-trimethyl-dodeca-2,6,10-triene-4-sulfonyl)-4-methyl-benzene

Guidance literature:: Multi-step reaction with 2 steps

2: 1.) n-BuLi, THF, HMPA, -40 to -30 deg C; 2.) -60 to 0 deg C / different sulphones investigated

With tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium;
DOI:10.1246/cl.1983.725

Reference yield:

: 15543-64-3
prenyl tolyl sulfone

: 86636-49-9
(2Z,6Z)-1-chloro-8-(benzyloxy)-2,6-dimethylocta-2,6-diene

: 86636-50-2
1-((6Z,10Z)-12-Benzyloxy-2,6,10-trimethyl-dodeca-2,6,10-triene-4-sulfonyl)-4-methyl-benzene

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1.) THF, HMPA, -40 to -30 deg C; 2.) -60 to 0 deg C;
DOI:10.1246/cl.1983.725