(E)-1-{2-hydroxy-4-methoxy-6-methoxymethoxy-3-[(1R,6R)-3-methyl-6-(1-methylethyl)-2-cyclohexen-1-yl]phenyl}-3-phenylprop-2-en-1-one

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Chemical Name:(E)-1-{2-hydroxy-4-methoxy-6-methoxymethoxy-3-[(1R,6R)-3-methyl-6-(1-methylethyl)-2-cyclohexen-1-yl]phenyl}-3-phenylprop-2-en-1-one
CAS No.:1273019-46-7
Molecular Formula:C₂₈H₃₄O₅
Molecular Weight:450.575
Hs Code.:

Synonyms:(E)-1-{2-hydroxy-4-methoxy-6-methoxymethoxy-3-[(1R,6R)-3-methyl-6-(1-methylethyl)-2-cyclohexen-1-yl]phenyl}-3-phenylprop-2-en-1-one

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Chemical Property of (E)-1-{2-hydroxy-4-methoxy-6-methoxymethoxy-3-[(1R,6R)-3-methyl-6-(1-methylethyl)-2-cyclohexen-1-yl]phenyl}-3-phenylprop-2-en-1-one

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Technology Process of (E)-1-{2-hydroxy-4-methoxy-6-methoxymethoxy-3-[(1R,6R)-3-methyl-6-(1-methylethyl)-2-cyclohexen-1-yl]phenyl}-3-phenylprop-2-en-1-one

There total 2 articles about (E)-1-{2-hydroxy-4-methoxy-6-methoxymethoxy-3-[(1R,6R)-3-methyl-6-(1-methylethyl)-2-cyclohexen-1-yl]phenyl}-3-phenylprop-2-en-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1273019-44-5
2'-hydroxy-4'-methoxy-6'-methoxymethoxy-3'-[(1R,6R)-3-methyl-6-(1-methylethyl)-2-cyclohexen-1-yl]acetophenone

: 100-52-7
benzaldehyde

: 1273019-46-7
(E)-1-{2-hydroxy-4-methoxy-6-methoxymethoxy-3-[(1R,6R)-3-methyl-6-(1-methylethyl)-2-cyclohexen-1-yl]phenyl}-3-phenylprop-2-en-1-one

Guidance literature:: With potassium tert-butylate; In tert-butyl alcohol; at 20 ℃; for 3.5h; Inert atmosphere;
DOI:10.3987/COM-10-12084

Reference yield:

: 1013913-57-9
1-{2,6-dihydroxy-4-methoxy-3-[(1R,6R)-3-methyl-6-(1-methylethyl)-2-cyclohexen-1-yl]phenyl}ethanone

: 1273019-46-7
(E)-1-{2-hydroxy-4-methoxy-6-methoxymethoxy-3-[(1R,6R)-3-methyl-6-(1-methylethyl)-2-cyclohexen-1-yl]phenyl}-3-phenylprop-2-en-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 0.5 h / Inert atmosphere; Reflux

2: potassium tert-butylate / tert-butyl alcohol / 3.5 h / 20 °C / Inert atmosphere

With potassium tert-butylate; potassium carbonate; In acetone; tert-butyl alcohol; 2: Aldol condensation;
DOI:10.3987/COM-10-12084

Reference yield: 67.0%

: 1273019-46-7
(E)-1-{2-hydroxy-4-methoxy-6-methoxymethoxy-3-[(1R,6R)-3-methyl-6-(1-methylethyl)-2-cyclohexen-1-yl]phenyl}-3-phenylprop-2-en-1-one

: 1273019-47-8
1-{2-hydroxy-4-methoxy-6-methoxymethoxy-3-[(1R,6R)-3-methyl-6-(1-methylethyl)-2-cyclohexen-1-yl]phenyl}-3-phenylpropan-1-one

Guidance literature:: (E)-1-{2-hydroxy-4-methoxy-6-methoxymethoxy-3-[(1R,6R)-3-methyl-6-(1-methylethyl)-2-cyclohexen-1-yl]phenyl}-3-phenylprop-2-en-1-one; With triethylsilane; Wilkinson's catalyst; In benzene; for 12h; Inert atmosphere; Reflux;

With hydrogenchloride; methanol; water; In water; benzene; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.3987/COM-10-12084