2-chloro-5-cyanobenzaldehyde chlorooxime

Base Information

Chemical Name:2-chloro-5-cyanobenzaldehyde chlorooxime
CAS No.:914106-05-1
Molecular Formula:C₈H₄Cl₂N₂O
Molecular Weight:215.039
Hs Code.:

Synonyms:2-chloro-5-cyanobenzaldehyde chlorooxime

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-chloro-5-cyanobenzaldehyde chlorooxime

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Technology Process of 2-chloro-5-cyanobenzaldehyde chlorooxime

There total 6 articles about 2-chloro-5-cyanobenzaldehyde chlorooxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 914106-41-5
5-cyano-2-chlorobenzaldoxime

: 914106-05-1
2-chloro-5-cyanobenzaldehyde chlorooxime

Guidance literature:: With N-chloro-succinimide; In N,N-dimethyl-formamide; at 25 ℃;
DOI:10.1021/jm0612867

Reference yield: 100.0%

: 914106-05-1
2-chloro-5-cyanobenzaldehyde chlorooxime

Guidance literature:

Reference yield:

: 89891-83-8
2-chloro-5-cyanobenzoic acid

: 914106-05-1
2-chloro-5-cyanobenzaldehyde chlorooxime

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / 1,3-dicyclohexylcarbodiimide / 4-dimethylaminopyridine / CH₂Cl₂ / 0 - 25 °C

2: 41 percent / pyrrolidine; t-BuOK; Red-Al / toluene; various solvent(s) / 0.25 h / 10 °C

3: 100 percent / hydroxylamine hydrochloride; pyridine / ethanol

4: 100 percent / N-chlorosuccinimide / dimethylformamide / 25 °C

With pyrrolidine; pyridine; N-chloro-succinimide; hydroxylamine hydrochloride; potassium tert-butylate; dicyclohexyl-carbodiimide; sodium bis(2-methoxyethoxy)aluminium dihydride; dmap; In ethanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm0612867