5-cyano-2-chlorobenzaldoxime

Base Information

Chemical Name:5-cyano-2-chlorobenzaldoxime
CAS No.:914106-41-5
Molecular Formula:C₈H₅ClN₂O
Molecular Weight:180.593
Hs Code.:

Synonyms:5-cyano-2-chlorobenzaldoxime

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Chemical Property of 5-cyano-2-chlorobenzaldoxime

Chemical Property:

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Technology Process of 5-cyano-2-chlorobenzaldoxime

There total 4 articles about 5-cyano-2-chlorobenzaldoxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 105191-41-1
4-chloro-3-formylbenzonitrile

: 914106-41-5
5-cyano-2-chlorobenzaldoxime

Guidance literature:: With pyridine; hydroxylamine hydrochloride; In ethanol;
DOI:10.1021/jm0612867

Reference yield:

: 89-54-3
2-chloro-5-aminobenzoic acid

: 914106-41-5
5-cyano-2-chlorobenzaldoxime

Guidance literature:: Multi-step reaction with 4 steps

1.1: NaNO₂; aq. HCl

1.2: KCN

2.1: 94 percent / 1,3-dicyclohexylcarbodiimide / 4-dimethylaminopyridine / CH₂Cl₂ / 0 - 25 °C

3.1: 41 percent / pyrrolidine; t-BuOK; Red-Al / toluene; various solvent(s) / 0.25 h / 10 °C

4.1: 100 percent / hydroxylamine hydrochloride; pyridine / ethanol

With pyrrolidine; pyridine; hydrogenchloride; hydroxylamine hydrochloride; potassium tert-butylate; dicyclohexyl-carbodiimide; sodium bis(2-methoxyethoxy)aluminium dihydride; sodium nitrite; dmap; In ethanol; dichloromethane; toluene; 1.2: Sandmeyer reaction;
DOI:10.1021/jm0612867

Reference yield:

: 89891-83-8
2-chloro-5-cyanobenzoic acid

: 914106-41-5
5-cyano-2-chlorobenzaldoxime

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / 1,3-dicyclohexylcarbodiimide / 4-dimethylaminopyridine / CH₂Cl₂ / 0 - 25 °C

2: 41 percent / pyrrolidine; t-BuOK; Red-Al / toluene; various solvent(s) / 0.25 h / 10 °C

3: 100 percent / hydroxylamine hydrochloride; pyridine / ethanol

With pyrrolidine; pyridine; hydroxylamine hydrochloride; potassium tert-butylate; dicyclohexyl-carbodiimide; sodium bis(2-methoxyethoxy)aluminium dihydride; dmap; In ethanol; dichloromethane; toluene;
DOI:10.1021/jm0612867