{4-[3-(dichloromethylene)hexyl]-3,5-dimethoxyphenyl}(pinacolato)borane

Base Information

Chemical Name:{4-[3-(dichloromethylene)hexyl]-3,5-dimethoxyphenyl}(pinacolato)borane
CAS No.:1060667-98-2
Molecular Formula:C₂₁H₃₁BCl₂O₄
Molecular Weight:429.192
Hs Code.:

Synonyms:{4-[3-(dichloromethylene)hexyl]-3,5-dimethoxyphenyl}(pinacolato)borane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {4-[3-(dichloromethylene)hexyl]-3,5-dimethoxyphenyl}(pinacolato)borane

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Technology Process of {4-[3-(dichloromethylene)hexyl]-3,5-dimethoxyphenyl}(pinacolato)borane

There total 1 articles about {4-[3-(dichloromethylene)hexyl]-3,5-dimethoxyphenyl}(pinacolato)borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1060667-97-1
2-[3-(dichloromethylene)hexyl]-1,3-dimethoxybenzene

: 73183-34-3
bis(pinacol)diborane

: 1060667-98-2
{4-[3-(dichloromethylene)hexyl]-3,5-dimethoxyphenyl}(pinacolato)borane

Guidance literature:: bis(pinacol)diborane; With [Ir(COD)(OMe)]₂; 4,4'-di-tert-butyl-2,2'-bipyridine; In hexane; at 20 ℃; for 0.25h;

2-[3-(dichloromethylene)hexyl]-1,3-dimethoxybenzene; at 150 ℃; for 3h; Microwave irradiation; Sealed vessel;
DOI:10.1055/s-2008-1078449

Reference yield: 97.0%

: 1060667-98-2
{4-[3-(dichloromethylene)hexyl]-3,5-dimethoxyphenyl}(pinacolato)borane

: 1060668-00-9
5-chloro-2-[3-(dichloromethylene)hexyl]-1,3-dimethoxybenzene

Guidance literature:: With copper(II) choride dihydrate; In water; isopropyl alcohol; at 150 ℃; for 2h; Microwave irradiation; Sealed vessel;
DOI:10.1055/s-2008-1078449