N-(2,2-diphenyl-1-chlorovinyl)-N-(dimethylaminodichloromethyl)-p-toluidine

Base Information

• Chemical Name: N-(2,2-diphenyl-1-chlorovinyl)-N-(dimethylaminodichloromethyl)-p-toluidine
• CAS No.: 91374-51-5
• Molecular Formula: C₂₄H₂₃Cl₃N₂
• Molecular Weight: 445.819
• Mol file: 91374-51-5.mol

Synonyms:N-(2,2-diphenyl-1-chlorovinyl)-N-(dimethylaminodichloromethyl)-p-toluidine

Chemical Property of N-(2,2-diphenyl-1-chlorovinyl)-N-(dimethylaminodichloromethyl)-p-toluidine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(2,2-diphenyl-1-chlorovinyl)-N-(dimethylaminodichloromethyl)-p-toluidine

There total 6 articles about N-(2,2-diphenyl-1-chlorovinyl)-N-(dimethylaminodichloromethyl)-p-toluidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

diphenylketene-N-p-tolylimine (5110-45-2,73940-93-9) + dichloromethylenedimethyliminium chloride (33842-02-3,529510-96-1) → N-(p-tolyl)diphenylacetamide (4107-01-1) + N-(2,2-diphenyl-1-chlorovinyl)-N-(dimethylaminodichloromethyl)-p-toluidine (91374-51-5)

Guidance literature:

In chloroform; for 48h; Ambient temperature;

Reference yield:

diphenylketene-N-p-tolylimine (5110-45-2,73940-93-9) → N-(2,2-diphenyl-1-chlorovinyl)-N-(dimethylaminodichloromethyl)-p-toluidine (91374-51-5)

Guidance literature:

Multi-step reaction with 2 steps

1: N,N-dimethyldichloromethyleneammonium chloride chlorine complex / CHCl₃

With Vilsmeier reagent; chlorine; In chloroform;

Reference yield:

2-chloro-2,2-diphenyl-N-p-tolyl-acetimidoyl chloride (5110-46-3) → N-(2,2-diphenyl-1-chlorovinyl)-N-(dimethylaminodichloromethyl)-p-toluidine (91374-51-5)

Guidance literature:

upstream raw materials:

diphenylketene-N-p-tolylimine

dichloromethylenedimethyliminium chloride

N-(p-tolyl)diphenylacetamide

2-chloro-2,2-diphenyl-N-p-tolyl-acetimidoyl chloride

Downstream raw materials:

N-(p-tolyl)diphenylacetamide

1-(2,2-diphenyl-1-chlorovinyl)-1-p-tolyl-2,2-dimethylurea