4-[4-(4-cyano-3-isopropylideneaminooxy-phenoxy)-butoxy]-N,N-diisopropyl-3-methoxy-benzamide

Base Information

Chemical Name:4-[4-(4-cyano-3-isopropylideneaminooxy-phenoxy)-butoxy]-N,N-diisopropyl-3-methoxy-benzamide
CAS No.:188658-65-3
Molecular Formula:C₂₈H₃₇N₃O₅
Molecular Weight:495.619
Hs Code.:

4-[4-(4-cyano-3-isopropylideneaminooxy-phenoxy)-butoxy]-<i>N</i>,<i>N</i>-diisopropyl-3-methoxy-benzamide

Synonyms:4-[4-(4-cyano-3-isopropylideneaminooxy-phenoxy)-butoxy]-N,N-diisopropyl-3-methoxy-benzamide

Suppliers and Price of 4-[4-(4-cyano-3-isopropylideneaminooxy-phenoxy)-butoxy]-N,N-diisopropyl-3-methoxy-benzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-[4-(4-cyano-3-isopropylideneaminooxy-phenoxy)-butoxy]-N,N-diisopropyl-3-methoxy-benzamide

Chemical Property:

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Technology Process of 4-[4-(4-cyano-3-isopropylideneaminooxy-phenoxy)-butoxy]-N,N-diisopropyl-3-methoxy-benzamide

There total 6 articles about 4-[4-(4-cyano-3-isopropylideneaminooxy-phenoxy)-butoxy]-N,N-diisopropyl-3-methoxy-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 188658-61-9
4-[4-(4-cyano-3-fluoro-phenoxy)-butoxy]-N,N-diisopropyl-3-methoxy-benzamide

: 127-06-0
acetone oxime

: 188658-65-3
4-[4-(4-cyano-3-isopropylideneaminooxy-phenoxy)-butoxy]-N,N-diisopropyl-3-methoxy-benzamide

Guidance literature:: With potassium tert-butylate; In N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(97)00025-5

Reference yield:

: 121-34-6
3-methoxy-4-hydroxybenzoic acid

: 188658-65-3
4-[4-(4-cyano-3-isopropylideneaminooxy-phenoxy)-butoxy]-N,N-diisopropyl-3-methoxy-benzamide

Guidance literature:: Multi-step reaction with 6 steps

1: thionyl chloride

3: 62 percent / potassium carbonate / acetonitrile

4: 66 percent / NaI / acetone

5: 56 percent / sodium hydride / dimethylformamide

6: 96 percent / potassium t-butoxide / dimethylformamide

With thionyl chloride; potassium tert-butylate; sodium hydride; potassium carbonate; sodium iodide; In N,N-dimethyl-formamide; acetone; acetonitrile; 1: Substitution / 2: Substitution / 3: Etherification / 4: Substitution / 5: Etherification / 6: Substitution;
DOI:10.1016/S0960-894X(97)00025-5

Reference yield:

: 55828-12-1
4-hydroxy-3-methoxy-benzoic acid chloride

: 188658-65-3
4-[4-(4-cyano-3-isopropylideneaminooxy-phenoxy)-butoxy]-N,N-diisopropyl-3-methoxy-benzamide

Guidance literature:: Multi-step reaction with 5 steps

2: 62 percent / potassium carbonate / acetonitrile

3: 66 percent / NaI / acetone

4: 56 percent / sodium hydride / dimethylformamide

5: 96 percent / potassium t-butoxide / dimethylformamide

With potassium tert-butylate; sodium hydride; potassium carbonate; sodium iodide; In N,N-dimethyl-formamide; acetone; acetonitrile; 1: Substitution / 2: Etherification / 3: Substitution / 4: Etherification / 5: Substitution;
DOI:10.1016/S0960-894X(97)00025-5