1,3-di(α-bromoacetyl)cresol

Base Information

Chemical Name:1,3-di(α-bromoacetyl)cresol
CAS No.:1431134-54-1
Molecular Formula:C₁₁H₁₀Br₂O₃
Molecular Weight:350.007
Hs Code.:

Synonyms:1,3-di(α-bromoacetyl)cresol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-di(α-bromoacetyl)cresol

Chemical Property:

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Technology Process of 1,3-di(α-bromoacetyl)cresol

There total 1 articles about 1,3-di(α-bromoacetyl)cresol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 55108-28-6
4-methyl-2,6-diacetylphenol

: 7726-95-6
bromine

: 1431134-54-1
1,3-di(α-bromoacetyl)cresol

Guidance literature:: In acetic acid; for 0.5h; Heating;
DOI:10.1039/c3dt00090g

Reference yield: 75.0%

: 5346-38-3
pyridine-2-carbothioamide

: 1431134-54-1
1,3-di(α-bromoacetyl)cresol

: C₂₃H₁₆N₄OS₂

Guidance literature:: In ethanol; at 60 ℃; for 12h; Inert atmosphere;
DOI:10.1039/c6ce02589g

Reference yield:

: 1431134-54-1
1,3-di(α-bromoacetyl)cresol

: C₃₁H₂₄N₄OS₂*Ag⁽¹⁺⁾*BF₄^(1-)

Guidance literature:: Multi-step reaction with 3 steps

1.1: ethanol / 12 h / 60 °C / Inert atmosphere

2.1: sodium hydride / mineral oil / 0.5 h / Inert atmosphere

2.2: 1 h / 80 °C / Inert atmosphere

2.3: 12 h / Inert atmosphere

3.1: nitromethane / Heating; Sonication

With sodium hydride; In nitromethane; ethanol; mineral oil;
DOI:10.1039/c6ce02589g