C₃₃H₅₄O₂S₂Si

Base Information

Chemical Name:C₃₃H₅₄O₂S₂Si
CAS No.:1375412-52-4
Molecular Formula:C₃₃H₅₄O₂S₂Si
Molecular Weight:575.008
Hs Code.:

C<sub>33</sub>H<sub>54</sub>O<sub>2</sub>S<sub>2</sub>Si

Synonyms:C₃₃H₅₄O₂S₂Si

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Chemical Property of C₃₃H₅₄O₂S₂Si

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Technology Process of C₃₃H₅₄O₂S₂Si

There total 7 articles about C₃₃H₅₄O₂S₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 105-87-3,8022-83-1
3,7-dimethyl-2E,6-octadien-1-yl acetate

: 1375412-52-4
C₃₃H₅₄O₂S₂Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 20 °C

2.1: copper(l) iodide / tetrahydrofuran; dimethyl sulfate / 3 h / -30 °C

3.1: sodium periodate / tetrahydrofuran; water / 6 h / 20 °C

4.1: N-chloro-succinimide; (2R,5S)-2-tert-butyl 3,5-dimethylimidazolidin-4-one trifluoroacetic acid salt / acetonitrile / 2.5 h / 0 °C

4.2: 0.5 h

5.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / 0 - 20 °C

5.2: 1 h / -50 - -45 °C

5.3: 2 h / -70 - 0 °C

With sodium periodate; N-chloro-succinimide; copper(l) iodide; n-butyllithium; (2R,5S)-2-tert-butyl 3,5-dimethylimidazolidin-4-one trifluoroacetic acid salt; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; hexane; dichloromethane; water; dimethyl sulfate; acetonitrile; 5.3: Brook rearrangement;
DOI:10.1002/anie.201108692

Reference yield:

: 758692-16-9
(E)-2,2-dimethyl-3-(3-methyl-5-phenylpent-3-enyl)oxirane

: 1375412-52-4
C₃₃H₅₄O₂S₂Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium periodate / tetrahydrofuran; water / 7.5 h / 20 °C

2.1: sodium hydride / tetrahydrofuran; dimethyl sulfoxide; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere

3.1: (1R,2R)-(-)-N,N'-bis(3,5-di-tert-butylsalicydene)-1,2-cyclohexanediaminocobalt(II); water; acetic acid / tetrahydrofuran / 17.5 h / 20 °C

4.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / 0 - 20 °C

4.2: 1 h / -50 - -45 °C

4.3: 2 h / -70 - 0 °C

With sodium periodate; (1R,2R)-(-)-N,N'-bis(3,5-di-tert-butylsalicydene)-1,2-cyclohexanediaminocobalt(II); n-butyllithium; water; sodium hydride; acetic acid; In tetrahydrofuran; hexane; water; dimethyl sulfoxide; mineral oil; 2.1: Corey-Chaykovsky reaction / 3.1: Jacobsen hydrolytic kinetic resolution / 4.3: Brook rearrangement;
DOI:10.1002/anie.201108692

Reference yield:

: 934672-43-2
(E)-4-methyl-6-phenylhex-4-enal

: 1375412-52-4
C₃₃H₅₄O₂S₂Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran; dimethyl sulfoxide; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere

2.1: (1R,2R)-(-)-N,N'-bis(3,5-di-tert-butylsalicydene)-1,2-cyclohexanediaminocobalt(II); water; acetic acid / tetrahydrofuran / 17.5 h / 20 °C

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / 0 - 20 °C

3.2: 1 h / -50 - -45 °C

3.3: 2 h / -70 - 0 °C

With (1R,2R)-(-)-N,N'-bis(3,5-di-tert-butylsalicydene)-1,2-cyclohexanediaminocobalt(II); n-butyllithium; water; sodium hydride; acetic acid; In tetrahydrofuran; hexane; dimethyl sulfoxide; mineral oil; 1.1: Corey-Chaykovsky reaction / 2.1: Jacobsen hydrolytic kinetic resolution / 3.3: Brook rearrangement;
DOI:10.1002/anie.201108692