(mercury)(benzaldehyde-N⁽⁴⁾,N⁽⁴⁾-dimethylthiosemicarbazone(-1H))2

Base Information

• Chemical Name: (mercury)(benzaldehyde-N⁽⁴⁾,N⁽⁴⁾-dimethylthiosemicarbazone(-1H))2
• CAS No.: 1227293-79-9
• Molecular Formula: C₂₀H₂₄HgN₆S₂
• Molecular Weight: 613.173
• Mol file: 1227293-79-9.mol

Synonyms:(mercury)(benzaldehyde-N⁽⁴⁾,N⁽⁴⁾-dimethylthiosemicarbazone(-1H))2

Chemical Property of (mercury)(benzaldehyde-N⁽⁴⁾,N⁽⁴⁾-dimethylthiosemicarbazone(-1H))2

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (mercury)(benzaldehyde-N⁽⁴⁾,N⁽⁴⁾-dimethylthiosemicarbazone(-1H))2

There total 4 articles about (mercury)(benzaldehyde-N⁽⁴⁾,N⁽⁴⁾-dimethylthiosemicarbazone(-1H))2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

mercuric(II) nitrate monohydrate + benzaldehyde-N(4),N(4)-dimethylthiosemicarbazone (2613-13-0) → (mercury)(benzaldehyde-N(4),N(4)-dimethylthiosemicarbazone(-1H))2 (1227293-79-9)

Guidance literature:

With LiOH*H₂O; In ethanol; EtOH soln. of semicarbazone deriv. with LiOH*H2O mixed with Hg(NO3)2*H2O; stirred at room temp. for 4 h; filtered, filtrate evapd. overnight; filtered off, washed with cold EtOHand Et2O, dried in vacuo;

DOI:10.1016/j.ica.2009.08.029

Reference yield:

benzaldehyde-N(4),N(4)-dimethylthiosemicarbazone (2613-13-0) + mercury(II) iodide → (mercury)(benzaldehyde-N(4),N(4)-dimethylthiosemicarbazone(-1H))2 (1227293-79-9)

Guidance literature:

With LiOH*H₂O; In ethanol; EtOH soln. of semicarbazone deriv. with LiOH*H2O mixed with HgI2; stirred at room temp. for 4 h; filtered, filtrate evapd. overnight; filtered off, washed with cold EtOHand Et2O, dried in vacuo;

DOI:10.1016/j.ica.2009.08.029

Reference yield:

benzaldehyde-N(4),N(4)-dimethylthiosemicarbazone (2613-13-0) + mercury dibromide → (mercury)(benzaldehyde-N(4),N(4)-dimethylthiosemicarbazone(-1H))2 (1227293-79-9)

Guidance literature:

With LiOH*H₂O; In ethanol; EtOH soln. of semicarbazone deriv. with LiOH*H2O mixed with HgBr2; stirred at room temp. for 4 h; filtered, filtrate evapd. overnight; filtered off, washed with cold EtOHand Et2O, dried in vacuo;

DOI:10.1016/j.ica.2009.08.029

upstream raw materials:

benzaldehyde-N⁽⁴⁾,N⁽⁴⁾-dimethylthiosemicarbazone