(Z)-N-((2S,4S,5R)-4-(benzyloxy)-5-((benzyloxy)methyl)-2-methoxydihydrofuran-3(2H)-ylidene)-2-methylpropane-2-sulfinamide

Base Information

Chemical Name:(Z)-N-((2S,4S,5R)-4-(benzyloxy)-5-((benzyloxy)methyl)-2-methoxydihydrofuran-3(2H)-ylidene)-2-methylpropane-2-sulfinamide
CAS No.:1439900-71-6
Molecular Formula:C₂₄H₃₁NO₅S
Molecular Weight:445.58
Hs Code.:

Synonyms:(Z)-N-((2S,4S,5R)-4-(benzyloxy)-5-((benzyloxy)methyl)-2-methoxydihydrofuran-3(2H)-ylidene)-2-methylpropane-2-sulfinamide

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Chemical Property of (Z)-N-((2S,4S,5R)-4-(benzyloxy)-5-((benzyloxy)methyl)-2-methoxydihydrofuran-3(2H)-ylidene)-2-methylpropane-2-sulfinamide

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Technology Process of (Z)-N-((2S,4S,5R)-4-(benzyloxy)-5-((benzyloxy)methyl)-2-methoxydihydrofuran-3(2H)-ylidene)-2-methylpropane-2-sulfinamide

There total 5 articles about (Z)-N-((2S,4S,5R)-4-(benzyloxy)-5-((benzyloxy)methyl)-2-methoxydihydrofuran-3(2H)-ylidene)-2-methylpropane-2-sulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 885592-69-8
(2S,4R,5R)-4-(benzyloxy)-5-((benzyloxy)methyl)-2-methoxydihydrofuran-3(2H)-one

: 146374-27-8
S-tert-butylsulfinimide

: 1439900-71-6
(Z)-N-((2S,4S,5R)-4-(benzyloxy)-5-((benzyloxy)methyl)-2-methoxydihydrofuran-3(2H)-ylidene)-2-methylpropane-2-sulfinamide

Guidance literature:: (2S,4R,5R)-4-(benzyloxy)-5-((benzyloxy)methyl)-2-methoxydihydrofuran-3(2H)-one; With titanium(IV) tetraethanolate; In tetrahydrofuran; at 20 ℃;

S-tert-butylsulfinimide; In tetrahydrofuran; at 60 ℃; for 6h;

Reference yield:

: 52485-92-4
methyl α-D-ribofuranoside

: 1439900-71-6
(Z)-N-((2S,4S,5R)-4-(benzyloxy)-5-((benzyloxy)methyl)-2-methoxydihydrofuran-3(2H)-ylidene)-2-methylpropane-2-sulfinamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.75 h / 0 °C

1.2: 16 h / 0 - 20 °C

2.1: tin(IV) chloride / dichloromethane / 24 h / 0 °C

3.1: Dess-Martin periodane / dichloromethane / 24 h / 0 - 20 °C

4.1: titanium(IV) tetraethanolate / tetrahydrofuran / 20 °C

4.2: 6 h / 60 °C

With titanium(IV) tetraethanolate; tin(IV) chloride; sodium hydride; Dess-Martin periodane; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 79083-29-7
(2R,3R,4R,5S)-3,4-bis(benzyloxy)-2-((benzyloxy)methyl)-5-methoxytetrahydrofuran

: 1439900-71-6
(Z)-N-((2S,4S,5R)-4-(benzyloxy)-5-((benzyloxy)methyl)-2-methoxydihydrofuran-3(2H)-ylidene)-2-methylpropane-2-sulfinamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: tin(IV) chloride / dichloromethane / 24 h / 0 °C

2.1: Dess-Martin periodane / dichloromethane / 24 h / 0 - 20 °C

3.1: titanium(IV) tetraethanolate / tetrahydrofuran / 20 °C

3.2: 6 h / 60 °C

With titanium(IV) tetraethanolate; tin(IV) chloride; Dess-Martin periodane; In tetrahydrofuran; dichloromethane;