Technology Process of 2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)indolo[3,2,1-jk]-carbazole
There total 1 articles about 2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)indolo[3,2,1-jk]-carbazole which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate; palladium diacetate; triphenylphosphine; ammonium bromide / N,N-dimethyl acetamide / 20 h / 150 °C
2: N-Bromosuccinimide / chloroform / 12 h / 0 - 20 °C
3: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 9 h / 80 °C
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; N-Bromosuccinimide; potassium acetate; palladium diacetate; potassium carbonate; ammonium bromide; triphenylphosphine;
In
1,4-dioxane; chloroform; N,N-dimethyl acetamide;
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); potassium carbonate;
In
ethanol; water; toluene;
at 110 ℃;
Inert atmosphere;
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); potassium carbonate;
In
ethanol; water; toluene;
at 100 ℃;
Inert atmosphere;
