(R)-2-Benzyloxymethoxymethyl-3-(tert-butyl-dimethyl-silanyloxy)-propionaldehyde

Base Information

Chemical Name:(R)-2-Benzyloxymethoxymethyl-3-(tert-butyl-dimethyl-silanyloxy)-propionaldehyde
CAS No.:133377-92-1
Molecular Formula:C₁₈H₃₀O₄Si
Molecular Weight:338.519
Hs Code.:

Synonyms:(R)-2-Benzyloxymethoxymethyl-3-(tert-butyl-dimethyl-silanyloxy)-propionaldehyde

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Chemical Property of (R)-2-Benzyloxymethoxymethyl-3-(tert-butyl-dimethyl-silanyloxy)-propionaldehyde

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Technology Process of (R)-2-Benzyloxymethoxymethyl-3-(tert-butyl-dimethyl-silanyloxy)-propionaldehyde

There total 10 articles about (R)-2-Benzyloxymethoxymethyl-3-(tert-butyl-dimethyl-silanyloxy)-propionaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3587-60-8
Benzyloxymethyl chloride

: 133377-92-1
(R)-2-Benzyloxymethoxymethyl-3-(tert-butyl-dimethyl-silanyloxy)-propionaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / EtN(iPr)2 / CH₂Cl₂ / a.) 0 deg C, 30 min, b.) room temperature, 6 h

2: ozone / methanol; CH₂Cl₂ / 2 h / Ambient temperature

With ozone; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane;
DOI:10.1021/jo00031a039

Reference yield:

: 138513-54-9
(R)-(E)-2-<<(Benzyloxy)methoxy>methyl>-1-<(tert-butyldimethylsilyl)oxy>-5-methylhex-3-ene

: 133377-92-1
(R)-2-Benzyloxymethoxymethyl-3-(tert-butyl-dimethyl-silanyloxy)-propionaldehyde

Guidance literature:: With dimethylsulfide; ozone; Multistep reaction; 1.) CH₂Cl₂, MeOH, -78 deg C, 2.) RT;
DOI:10.1016/S0957-4166(00)82383-6

Reference yield:

: 226926-94-9
Acetic acid (E)-(R)-2-(tert-butyl-dimethyl-silanyloxymethyl)-5-methyl-hex-3-enyl ester

: 133377-92-1
(R)-2-Benzyloxymethoxymethyl-3-(tert-butyl-dimethyl-silanyloxy)-propionaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 0.1 N KOH/MeOH

2: 86 percent / EtN(i-Pr)2 / CH₂Cl₂ / Ambient temperature

3: 1) O₃, 2) Me₂S / 1) CH₂Cl₂/MeOH, -78 deg C, 2) room temp., 5 h

With methanol; potassium hydroxide; dimethylsulfide; ozone; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1016/S0040-4039(00)97081-3