N-(4,6-dichloro-1,3,5-triazin-2-yl)-L-4-(N,N-dimethylcarbamyloxy)-phenylalanine tert-butyl ester

Base Information

• Chemical Name: N-(4,6-dichloro-1,3,5-triazin-2-yl)-L-4-(N,N-dimethylcarbamyloxy)-phenylalanine tert-butyl ester
• CAS No.: 285562-31-4
• Molecular Formula: C₁₉H₂₃Cl₂N₅O₄
• Molecular Weight: 456.329

Synonyms:N-(4,6-dichloro-1,3,5-triazin-2-yl)-L-4-(N,N-dimethylcarbamyloxy)-phenylalanine tert-butyl ester

Chemical Property of N-(4,6-dichloro-1,3,5-triazin-2-yl)-L-4-(N,N-dimethylcarbamyloxy)-phenylalanine tert-butyl ester

Chemical Property:

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Technology Process of N-(4,6-dichloro-1,3,5-triazin-2-yl)-L-4-(N,N-dimethylcarbamyloxy)-phenylalanine tert-butyl ester

There total 1 articles about N-(4,6-dichloro-1,3,5-triazin-2-yl)-L-4-(N,N-dimethylcarbamyloxy)-phenylalanine tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3,5-trichloro-2,4,6-triazine (108-77-0) + L-4-(N,N-dimethylcarbamyloxy)phenylalanine tert-butyl ester (284486-57-3) → N-(4,6-dichloro-1,3,5-triazin-2-yl)-L-4-(N,N-dimethylcarbamyloxy)-phenylalanine tert-butyl ester (285562-31-4)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran;

Reference yield:

N-(4,6-dichloro-1,3,5-triazin-2-yl)-L-4-(N,N-dimethylcarbamyloxy)-phenylalanine tert-butyl ester (285562-31-4) + N-methyl-p-toluenesulfonylamide (640-61-9) → N-{4-chloro-6-[N-(methyl)-N-(p-toluenesulfonyl)amino]-1,3,5-triazin-2-yl}-L-4-(N,N-dimethylcarbamyloxy)-phenylalanine tert-butyl ester (285562-33-6)

Guidance literature:

With caesium carbonate; In tetrahydrofuran;

Reference yield:

N-(4,6-dichloro-1,3,5-triazin-2-yl)-L-4-(N,N-dimethylcarbamyloxy)-phenylalanine tert-butyl ester (285562-31-4) + N-benzyl-2-phenylethylamine (3647-71-0) → N-{6-[N-(benzyl)-N-(1-phenylethyl)amino]-4-chloro-1,3,5-triazin-2-yl}-L-4-(N,N-dimethylcarbamyloxy)phenylalanine tert-butyl ester (285562-32-5)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran;

upstream raw materials:

1,3,5-trichloro-2,4,6-triazine

L-4-(N,N-dimethylcarbamyloxy)phenylalanine tert-butyl ester

Downstream raw materials:

N-{4-chloro-6-[N-(methyl)-N-(p-toluenesulfonyl)amino]-1,3,5-triazin-2-yl}-L-4-(N,N-dimethylcarbamyloxy)-phenylalanine tert-butyl ester

N-{6-[N-(benzyl)-N-(1-phenylethyl)amino]-4-chloro-1,3,5-triazin-2-yl}-L-4-(N,N-dimethylcarbamyloxy)phenylalanine tert-butyl ester

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