1<(1',2'-dideoxy-3',4';5',6'-di-O-isopropylidene-1'(1,3-propanedithio))-D-2'-glucosyl>-3,3-diethyl-4α-(α-methylstyryl)-2-azetidinone

Base Information

Chemical Name:1<(1',2'-dideoxy-3',4';5',6'-di-O-isopropylidene-1'(1,3-propanedithio))-D-2'-glucosyl>-3,3-diethyl-4α-(α-methylstyryl)-2-azetidinone
CAS No.:241156-07-0
Molecular Formula:C₃₁H₄₅NO₅S₂
Molecular Weight:575.834
Hs Code.:

Synonyms:1<(1',2'-dideoxy-3',4';5',6'-di-O-isopropylidene-1'(1,3-propanedithio))-D-2'-glucosyl>-3,3-diethyl-4α-(α-methylstyryl)-2-azetidinone

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Chemical Property of 1<(1',2'-dideoxy-3',4';5',6'-di-O-isopropylidene-1'(1,3-propanedithio))-D-2'-glucosyl>-3,3-diethyl-4α-(α-methylstyryl)-2-azetidinone

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Technology Process of 1<(1',2'-dideoxy-3',4';5',6'-di-O-isopropylidene-1'(1,3-propanedithio))-D-2'-glucosyl>-3,3-diethyl-4α-(α-methylstyryl)-2-azetidinone

There total 3 articles about 1<(1',2'-dideoxy-3',4';5',6'-di-O-isopropylidene-1'(1,3-propanedithio))-D-2'-glucosyl>-3,3-diethyl-4α-(α-methylstyryl)-2-azetidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2736-40-5
chlorure d'acide ethyl-2 butyrique

: [(R)-[1,3]Dithian-2-yl-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-methyl]-[(E)-2-methyl-3-phenyl-prop-2-en-(E)-ylidene]-amine

: 241156-29-6
1<(1',2'-dideoxy-3',4';5',6'-di-O-isopropylidene-1'(1,3-propanedithio))-D-2'-glucosyl>-3,3-diethyl-4β-(α-methylstyryl)-2-azetidinone

: 241156-07-0
1<(1',2'-dideoxy-3',4';5',6'-di-O-isopropylidene-1'(1,3-propanedithio))-D-2'-glucosyl>-3,3-diethyl-4α-(α-methylstyryl)-2-azetidinone

Guidance literature:: With TEA; In toluene; at 50 ℃; for 10h; Yield given; Yields of byproduct given;
DOI:10.1016/S0968-0896(98)00264-8

Reference yield:

: 135565-72-9
2-amino-2-deoxy-D-glucose propane-1,3-diyldithioacetal

: 241156-07-0
1<(1',2'-dideoxy-3',4';5',6'-di-O-isopropylidene-1'(1,3-propanedithio))-D-2'-glucosyl>-3,3-diethyl-4α-(α-methylstyryl)-2-azetidinone

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / p-TsOH / 3 h / 60 °C

2: toluene / 5 h / 70 °C

3: TEA / toluene / 10 h / 50 °C

With TEA; toluene-4-sulfonic acid; In toluene;
DOI:10.1016/S0968-0896(98)00264-8

Reference yield:

: 66-84-2
D-(+)-glucosamine hydrochloride

: 241156-07-0
1<(1',2'-dideoxy-3',4';5',6'-di-O-isopropylidene-1'(1,3-propanedithio))-D-2'-glucosyl>-3,3-diethyl-4α-(α-methylstyryl)-2-azetidinone

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / HCl / aq. HCl; CH₂Cl₂ / 12 h / 60 °C

2: 90 percent / p-TsOH / 3 h / 60 °C

3: toluene / 5 h / 70 °C

4: TEA / toluene / 10 h / 50 °C

With hydrogenchloride; TEA; toluene-4-sulfonic acid; In hydrogenchloride; dichloromethane; toluene;
DOI:10.1016/S0968-0896(98)00264-8