K₁(O)-[(carbonyl)3 (bis(diphenylphosphino)ethan) (pyridine-3-carboxylate) manganese(I)]

Base Information

• Chemical Name: K₁(O)-[(carbonyl)3 (bis(diphenylphosphino)ethan) (pyridine-3-carboxylate) manganese(I)]
• CAS No.: 885008-58-2
• Molecular Formula: C₃₅H₂₈MnNO₅P₂
• Molecular Weight: 659.497

Synonyms:K₁(O)-[(carbonyl)3 (bis(diphenylphosphino)ethan) (pyridine-3-carboxylate) manganese(I)]

Chemical Property of K₁(O)-[(carbonyl)3 (bis(diphenylphosphino)ethan) (pyridine-3-carboxylate) manganese(I)]

Chemical Property:

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Technology Process of K₁(O)-[(carbonyl)3 (bis(diphenylphosphino)ethan) (pyridine-3-carboxylate) manganese(I)]

There total 1 articles about K₁(O)-[(carbonyl)3 (bis(diphenylphosphino)ethan) (pyridine-3-carboxylate) manganese(I)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

nicotinic acid (59-67-6) + [fac-Mn(CO)3(1,2-bis(diphenylphosphino)ethane)(OH2)]BF4 (247939-31-7) → K1(O)-[(carbonyl)3 (bis(diphenylphosphino)ethan) (pyridine-3-carboxylate) manganese(I)] (885008-58-2)

Guidance literature:

With sodium hydroxide; In chloroform; water; (Ar); aq. NaOH soln. of nicotinic acid added dropwise to CHCl3 soln. of (CO)3(dppe)Mn(OH2)BF4 in equimolar quantity; stirring continued for 10-20 min; CHCl3 soln. separated; washed with water; dried and evaporated; resulting solid washed with hexane; dried in vacuo;

DOI:10.1016/j.poly.2005.08.032

upstream raw materials:

nicotinic acid

[fac-Mn(CO)3(1,2-bis(diphenylphosphino)ethane)(OH₂)]BF₄

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