C₃₆H₃₇N₃O₁₀

Base Information

Chemical Name:C₃₆H₃₇N₃O₁₀
CAS No.:1196977-89-5
Molecular Formula:C₃₆H₃₇N₃O₁₀
Molecular Weight:671.704
Hs Code.:

C<sub>36</sub>H<sub>37</sub>N<sub>3</sub>O<sub>10</sub>

Synonyms:C₃₆H₃₇N₃O₁₀

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₆H₃₇N₃O₁₀

Chemical Property:

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Technology Process of C₃₆H₃₇N₃O₁₀

There total 10 articles about C₃₆H₃₇N₃O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1196977-88-4
C₃₅H₃₅N₃O₁₀

: 74-88-4
methyl iodide

: 1196977-89-5
C₃₆H₃₇N₃O₁₀

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/anie.200904588

Reference yield:

: 1276541-17-3
C₇H₇NO₃

: 1196977-89-5
C₃₆H₃₇N₃O₁₀

Guidance literature:: Multi-step reaction with 6 steps

1.1: trifluorormethanesulfonic acid / dichloromethane / 2 h / -78 - 0 °C

2.1: triethylamine / dichloromethane / 1 h / 23 °C

3.1: 1,1'-bis-(diphenylphosphino)ferrocene; formic acid; tributylsilane; palladium diacetate; triethylamine / N,N-dimethyl-formamide / 1 h / 50 °C

4.1: sulfuryl dichloride / dichloromethane / -78 - 20 °C

4.2: 1 h / 20 °C

5.1: borane-THF / tetrahydrofuran / 7 h / 0 °C

6.1: dmap; triethylamine / dichloromethane

With dmap; 1,1'-bis-(diphenylphosphino)ferrocene; formic acid; sulfuryl dichloride; borane-THF; tributylsilane; trifluorormethanesulfonic acid; palladium diacetate; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 3.1: Gassman synthesis;
DOI:10.1002/ejoc.201001629

Reference yield:

: 1276541-24-2
C₇H₉NO₃

: 1196977-89-5
C₃₆H₃₇N₃O₁₀

Guidance literature:: Multi-step reaction with 7 steps

1.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / ethyl acetate / 0.08 h / 20 °C

2.1: trifluorormethanesulfonic acid / dichloromethane / 2 h / -78 - 0 °C

3.1: triethylamine / dichloromethane / 1 h / 23 °C

4.1: 1,1'-bis-(diphenylphosphino)ferrocene; formic acid; tributylsilane; palladium diacetate; triethylamine / N,N-dimethyl-formamide / 1 h / 50 °C

5.1: sulfuryl dichloride / dichloromethane / -78 - 20 °C

5.2: 1 h / 20 °C

6.1: borane-THF / tetrahydrofuran / 7 h / 0 °C

7.1: dmap; triethylamine / dichloromethane

With dmap; 1,1'-bis-(diphenylphosphino)ferrocene; formic acid; sulfuryl dichloride; borane-THF; tributylsilane; trifluorormethanesulfonic acid; palladium diacetate; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; 4.1: Gassman synthesis;
DOI:10.1002/ejoc.201001629