(3α,4β)-3-ethenyl-4--4-methyl-2-methylenecyclohexanone

Base Information

Chemical Name:(3α,4β)-3-ethenyl-4--4-methyl-2-methylenecyclohexanone
CAS No.:126724-81-0
Molecular Formula:C₂₁H₃₆O₃
Molecular Weight:336.515
Hs Code.:

(3α,4β)-3-ethenyl-4-<bis(1-ethylpropoxy)methyl>-4-methyl-2-methylenecyclohexanone

Synonyms:(3α,4β)-3-ethenyl-4--4-methyl-2-methylenecyclohexanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3α,4β)-3-ethenyl-4--4-methyl-2-methylenecyclohexanone

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Technology Process of (3α,4β)-3-ethenyl-4--4-methyl-2-methylenecyclohexanone

There total 3 articles about (3α,4β)-3-ethenyl-4--4-methyl-2-methylenecyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 126724-80-9
(2α,3β,4α)-3-ethenyl-4--4-methyl-2-<<(methysulfonyl)oxy>methyl>cyclohexanone

: 126724-81-0
(3α,4β)-3-ethenyl-4--4-methyl-2-methylenecyclohexanone

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In benzene; for 1h; Ambient temperature;
DOI:10.1021/jo00299a048

Reference yield:

: 126395-39-9
4-[Bis-(1-ethyl-propoxy)-methyl]-4-methyl-cyclohex-2-enone

: 126724-81-0
(3α,4β)-3-ethenyl-4--4-methyl-2-methylenecyclohexanone

Guidance literature:: Multi-step reaction with 3 steps

2: Et₃N / CH₂Cl₂ / 3.5 h / 0 °C

3: 90 percent / DBU / benzene / 1 h / Ambient temperature

With 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In dichloromethane; benzene;
DOI:10.1021/jo00299a048

Reference yield:

: 126786-76-3
(2α,3β,4α)-3-ethenyl-4--2-(hydroxymethyl)-4-methylcyclohexanone

: 126724-81-0
(3α,4β)-3-ethenyl-4--4-methyl-2-methylenecyclohexanone

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 3.5 h / 0 °C

2: 90 percent / DBU / benzene / 1 h / Ambient temperature

With 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In dichloromethane; benzene;
DOI:10.1021/jo00299a048