3-phenanthroylmethyl pyridinium bromide

Base Information

• Chemical Name: 3-phenanthroylmethyl pyridinium bromide
• CAS No.: 76734-07-1
• Molecular Formula: Br*C₂₁H₁₆NO
• Molecular Weight: 378.268

Synonyms:3-phenanthroylmethyl pyridinium bromide

Chemical Property of 3-phenanthroylmethyl pyridinium bromide

Chemical Property:

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Technology Process of 3-phenanthroylmethyl pyridinium bromide

There total 1 articles about 3-phenanthroylmethyl pyridinium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

pyridine (110-86-1) + 2-bromo-3'-acetophenanthrone (34585-56-3) → 3-phenanthroylmethyl pyridinium bromide (76734-07-1)

Guidance literature:

With ethanol;

Reference yield: 75.0%

3-phenanthroylmethyl pyridinium bromide (76734-07-1) + (E)-3-(benzo[d][1,3]dioxol-5-yl)-1-(4-bromophenyl)prop-2-en-1-one (36716-01-5) → 4-benzo[1,3]dioxol-5-yl-2-(4-bromo-phenyl)-6-phenanthren-3-yl-pyridine (62953-33-7)

Guidance literature:

With ammonium acetate; In acetic acid; at 120 ℃;

Reference yield: 65.0%

(2E)-3-(4-chlorophenyl)-1-naphthalen-2-yl-prop-2-en-1-one (62918-41-6) + 3-phenanthroylmethyl pyridinium bromide (76734-07-1) → 4-(4-Chloro-phenyl)-2-naphthalen-2-yl-6-phenanthren-3-yl-pyridine

Guidance literature:

With ammonium acetate; In acetic acid; at 120 ℃;

upstream raw materials:

pyridine

2-bromo-3'-acetophenanthrone

Downstream raw materials:

4-(4-chloro-phenyl)-2-phenanthren-3-yl-6-p-tolyl-pyridine

4-(2,4-dichloro-phenyl)-2-phenanthren-3-yl-6-p-tolyl-pyridine

4-benzo[1,3]dioxol-5-yl-2-(4-bromo-phenyl)-6-phenanthren-3-yl-pyridine

4-(2,4-dichloro-phenyl)-2-naphthalen-2-yl-6-phenanthren-3-yl-pyridine

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