Technology Process of 1,1'-Dimethyl-2,3,2',3'-tetraphenyl-3H,1'H-[3,6']biindolyl-1-ium; perchlorate
There total 3 articles about 1,1'-Dimethyl-2,3,2',3'-tetraphenyl-3H,1'H-[3,6']biindolyl-1-ium; perchlorate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetraethylammonium perchlorate;
In
acetonitrile;
electrochemical oxidation;
DOI:10.1021/jo00232a042
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) conc. HCl / 1.) reflux, 35 min, 2.) from 175 to 185 deg C, 1 h
2: 60 percent / tetraethylammonium perchlorate (TEAP) / acetonitrile / electrochemical oxidation
With
hydrogenchloride; tetraethylammonium perchlorate;
In
acetonitrile;
DOI:10.1021/jo00232a042
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) conc. HCl / 1.) reflux, 35 min, 2.) from 175 to 185 deg C, 1 h
2: 60 percent / tetraethylammonium perchlorate (TEAP) / acetonitrile / electrochemical oxidation
With
hydrogenchloride; tetraethylammonium perchlorate;
In
acetonitrile;
DOI:10.1021/jo00232a042