C-(2-Benzyl-5,7,8-trimethoxy-6-methyl-1,2,3,4-tetrahydro-isoquinolin-1-yl)-methylamine

Base Information

Chemical Name:C-(2-Benzyl-5,7,8-trimethoxy-6-methyl-1,2,3,4-tetrahydro-isoquinolin-1-yl)-methylamine
CAS No.:124867-39-6
Molecular Formula:C₂₁H₂₈N₂O₃
Molecular Weight:356.465
Hs Code.:

Synonyms:C-(2-Benzyl-5,7,8-trimethoxy-6-methyl-1,2,3,4-tetrahydro-isoquinolin-1-yl)-methylamine

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Chemical Property of C-(2-Benzyl-5,7,8-trimethoxy-6-methyl-1,2,3,4-tetrahydro-isoquinolin-1-yl)-methylamine

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Technology Process of C-(2-Benzyl-5,7,8-trimethoxy-6-methyl-1,2,3,4-tetrahydro-isoquinolin-1-yl)-methylamine

There total 5 articles about C-(2-Benzyl-5,7,8-trimethoxy-6-methyl-1,2,3,4-tetrahydro-isoquinolin-1-yl)-methylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124867-38-5
2-Benzyl-6-methyl-5,7,8-trimethoxy-1-phthalimidomethyl-1,2,3,4-tetrahydroisoquinoline

: 124867-39-6
C-(2-Benzyl-5,7,8-trimethoxy-6-methyl-1,2,3,4-tetrahydro-isoquinolin-1-yl)-methylamine

Guidance literature:: With hydrazine hydrate; In ethanol; for 2h; Yield given; Heating;
DOI:10.1248/cpb.37.1493

Reference yield:

: 113966-96-4
N-Benzyl-2-(2,4,5-trimethoxy-3-methylphenyl)ethylamine

: 124867-39-6
C-(2-Benzyl-5,7,8-trimethoxy-6-methyl-1,2,3,4-tetrahydro-isoquinolin-1-yl)-methylamine

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / Ambient temperature

2: trifluoroacetic acid / 1 h / Ambient temperature

3: 72 percent / lithium aluminium hydride / tetrahydrofuran / 2 h / Heating

4: 86 percent / diethyl azodicarboxylate, triphenylphosphine / tetrahydrofuran / 2 h / Ambient temperature

5: hydrazine monohydrate / ethanol / 2 h / Heating

With lithium aluminium tetrahydride; potassium carbonate; hydrazine hydrate; triphenylphosphine; trifluoroacetic acid; diethylazodicarboxylate; In tetrahydrofuran; ethanol;
DOI:10.1248/cpb.37.1493

Reference yield:

: 113967-11-6
Butyl 2-benzyl-5,7,8-trimethoxy-6-methyl-1,2,3,4-tetrahydroisoquinoline-1-carboxylate

: 124867-39-6
C-(2-Benzyl-5,7,8-trimethoxy-6-methyl-1,2,3,4-tetrahydro-isoquinolin-1-yl)-methylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / lithium aluminium hydride / tetrahydrofuran / 2 h / Heating

2: 86 percent / diethyl azodicarboxylate, triphenylphosphine / tetrahydrofuran / 2 h / Ambient temperature

3: hydrazine monohydrate / ethanol / 2 h / Heating

With lithium aluminium tetrahydride; hydrazine hydrate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; ethanol;
DOI:10.1248/cpb.37.1493