2-Benzyl-1-hydroxymethyl-6-metyl-5,7,8-trimethoxy-1,2,3,4-tetrahydroisoquinoline

Base Information

Chemical Name:2-Benzyl-1-hydroxymethyl-6-metyl-5,7,8-trimethoxy-1,2,3,4-tetrahydroisoquinoline
CAS No.:124867-37-4
Molecular Formula:C₂₁H₂₇NO₄
Molecular Weight:357.45
Hs Code.:

Synonyms:2-Benzyl-1-hydroxymethyl-6-metyl-5,7,8-trimethoxy-1,2,3,4-tetrahydroisoquinoline

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Chemical Property of 2-Benzyl-1-hydroxymethyl-6-metyl-5,7,8-trimethoxy-1,2,3,4-tetrahydroisoquinoline

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Technology Process of 2-Benzyl-1-hydroxymethyl-6-metyl-5,7,8-trimethoxy-1,2,3,4-tetrahydroisoquinoline

There total 3 articles about 2-Benzyl-1-hydroxymethyl-6-metyl-5,7,8-trimethoxy-1,2,3,4-tetrahydroisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 113967-11-6
Butyl 2-benzyl-5,7,8-trimethoxy-6-methyl-1,2,3,4-tetrahydroisoquinoline-1-carboxylate

: 124867-37-4
2-Benzyl-1-hydroxymethyl-6-metyl-5,7,8-trimethoxy-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 2h; Heating;
DOI:10.1248/cpb.37.1493

Reference yield:

: 113966-96-4
N-Benzyl-2-(2,4,5-trimethoxy-3-methylphenyl)ethylamine

: 124867-37-4
2-Benzyl-1-hydroxymethyl-6-metyl-5,7,8-trimethoxy-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / Ambient temperature

2: trifluoroacetic acid / 1 h / Ambient temperature

3: 72 percent / lithium aluminium hydride / tetrahydrofuran / 2 h / Heating

With lithium aluminium tetrahydride; potassium carbonate; trifluoroacetic acid; In tetrahydrofuran;
DOI:10.1248/cpb.37.1493

Reference yield:

: 124867-32-9
{Benzyl-[2-(2,4,5-trimethoxy-3-methyl-phenyl)-ethyl]-amino}-butoxy-acetic acid butyl ester

: 124867-37-4
2-Benzyl-1-hydroxymethyl-6-metyl-5,7,8-trimethoxy-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / 1 h / Ambient temperature

2: 72 percent / lithium aluminium hydride / tetrahydrofuran / 2 h / Heating

With lithium aluminium tetrahydride; trifluoroacetic acid; In tetrahydrofuran;
DOI:10.1248/cpb.37.1493