N-Benzyl-N-[(1R)-1-(tert-butyl(dimethyl)siloxymethyl)prop-2-enyl]-N-[(2Z)-3-methyl-4-phenoxybut-2-enyl]amine

Base Information

Chemical Name:N-Benzyl-N-[(1R)-1-(tert-butyl(dimethyl)siloxymethyl)prop-2-enyl]-N-[(2Z)-3-methyl-4-phenoxybut-2-enyl]amine
CAS No.:313995-42-5
Molecular Formula:C₂₈H₄₁NO₂Si
Molecular Weight:451.725
Hs Code.:

Synonyms:N-Benzyl-N-[(1R)-1-(tert-butyl(dimethyl)siloxymethyl)prop-2-enyl]-N-[(2Z)-3-methyl-4-phenoxybut-2-enyl]amine

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Chemical Property of N-Benzyl-N-[(1R)-1-(tert-butyl(dimethyl)siloxymethyl)prop-2-enyl]-N-[(2Z)-3-methyl-4-phenoxybut-2-enyl]amine

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Technology Process of N-Benzyl-N-[(1R)-1-(tert-butyl(dimethyl)siloxymethyl)prop-2-enyl]-N-[(2Z)-3-methyl-4-phenoxybut-2-enyl]amine

There total 7 articles about N-Benzyl-N-[(1R)-1-(tert-butyl(dimethyl)siloxymethyl)prop-2-enyl]-N-[(2Z)-3-methyl-4-phenoxybut-2-enyl]amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 221662-33-5
{[(2Z)-4-Chloro-2-methylbut-2-enyl]oxy}benzene

: 313995-41-4
(-)-(2R)-N-benzyl-1-(tert-butyldimethylsiloxy)but-3-en-2-amine

: 313995-42-5
N-Benzyl-N-[(1R)-1-(tert-butyl(dimethyl)siloxymethyl)prop-2-enyl]-N-[(2Z)-3-methyl-4-phenoxybut-2-enyl]amine

Guidance literature:: With potassium carbonate; sodium iodide; In acetonitrile; Heating;
DOI:10.1039/b005853j

Reference yield:

: 621-87-4
3-phenoxy-2-propanone

: 313995-42-5
N-Benzyl-N-[(1R)-1-(tert-butyl(dimethyl)siloxymethyl)prop-2-enyl]-N-[(2Z)-3-methyl-4-phenoxybut-2-enyl]amine

Guidance literature:: Multi-step reaction with 4 steps

1.1: NaH / tetrahydrofuran / 0.5 h

1.2: 32 percent / tetrahydrofuran / 0.5 h / -15 °C

2.1: DIBAL / toluene / 0.5 h / -78 °C

3.1: 372 mg / TsCl; DMAP / CH₂Cl₂

4.1: 86 percent / K₂CO₃; NaI / acetonitrile / Heating

With dmap; sodium hydride; diisobutylaluminium hydride; potassium carbonate; p-toluenesulfonyl chloride; sodium iodide; In tetrahydrofuran; dichloromethane; toluene; acetonitrile; 1.1: Metallation / 1.2: Condensation / 2.1: Reduction / 3.1: Substitution / 4.1: Alkylation;
DOI:10.1039/b005853j

Reference yield:

: 100-52-7
benzaldehyde

: 313995-42-5
N-Benzyl-N-[(1R)-1-(tert-butyl(dimethyl)siloxymethyl)prop-2-enyl]-N-[(2Z)-3-methyl-4-phenoxybut-2-enyl]amine

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N; Na₂SO₄ / CH₂Cl₂ / Heating

2: NaBH₄ / methanol / 1 h / 20 °C

3: 900 mg / imidazole / dimethylformamide

4: 86 percent / K₂CO₃; NaI / acetonitrile / Heating

With 1H-imidazole; sodium tetrahydroborate; potassium carbonate; sodium sulfate; triethylamine; sodium iodide; In methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 1: Condensation / 2: Reduction / 3: Etherification / 4: Alkylation;
DOI:10.1039/b005853j