(4-(4-(((6-methoxy-2-(2-methoxyimidazo[2,1-b][1,3,4]thiadiazol-6-yl)benzofuran-4-yl)oxy)methyl)-5-methylthiazol-2-yl)morpholine)

Base Information

Chemical Name:(4-(4-(((6-methoxy-2-(2-methoxyimidazo[2,1-b][1,3,4]thiadiazol-6-yl)benzofuran-4-yl)oxy)methyl)-5-methylthiazol-2-yl)morpholine)
CAS No.:1476847-58-1
Molecular Formula:C₂₄H₁₈N₄O₄S₂
Molecular Weight:490.563
Hs Code.:

Synonyms:(4-(4-(((6-methoxy-2-(2-methoxyimidazo[2,1-b][1,3,4]thiadiazol-6-yl)benzofuran-4-yl)oxy)methyl)-5-methylthiazol-2-yl)morpholine)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4-(4-(((6-methoxy-2-(2-methoxyimidazo[2,1-b][1,3,4]thiadiazol-6-yl)benzofuran-4-yl)oxy)methyl)-5-methylthiazol-2-yl)morpholine)

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (4-(4-(((6-methoxy-2-(2-methoxyimidazo[2,1-b][1,3,4]thiadiazol-6-yl)benzofuran-4-yl)oxy)methyl)-5-methylthiazol-2-yl)morpholine)

There total 8 articles about (4-(4-(((6-methoxy-2-(2-methoxyimidazo[2,1-b][1,3,4]thiadiazol-6-yl)benzofuran-4-yl)oxy)methyl)-5-methylthiazol-2-yl)morpholine) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 23780-13-4
(2-phenylthiazol-4-yl)methanol

: 1476847-56-9
6-methoxy-2-(2-methoxyimidazolo[2,1-b][1,3,4]thiadiazol-6-yl)benzofuran-4-ol

: 1476847-58-1
(4-(4-(((6-methoxy-2-(2-methoxyimidazo[2,1-b][1,3,4]thiadiazol-6-yl)benzofuran-4-yl)oxy)methyl)-5-methylthiazol-2-yl)morpholine)

Guidance literature:: (2-phenylthiazol-4-yl)methanol; 6-methoxy-2-(2-methoxyimidazolo[2,1-b][1,3,4]thiadiazol-6-yl)benzofuran-4-ol; With lithium aluminium tetrahydride; triphenylphosphine; In tetrahydrofuran; at 50 ℃; for 0.0833333h; Inert atmosphere; Sonication;

With di-isopropyl azodicarboxylate; In tetrahydrofuran; at 22 ℃; for 5h; Inert atmosphere;

Reference yield:

: ethyl acetate dichloromethane

: 23780-13-4
(2-phenylthiazol-4-yl)methanol

: 1476847-56-9
6-methoxy-2-(2-methoxyimidazolo[2,1-b][1,3,4]thiadiazol-6-yl)benzofuran-4-ol

: 1476847-58-1
(4-(4-(((6-methoxy-2-(2-methoxyimidazo[2,1-b][1,3,4]thiadiazol-6-yl)benzofuran-4-yl)oxy)methyl)-5-methylthiazol-2-yl)morpholine)

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran;

Reference yield:

: 1476847-55-8
6-(4-(benzyloxy)-6-methoxybenzofuran-2-yl)-2-methoxyimidazo[2,1-b][1,3,4]thiadiazole

: 1476847-58-1
(4-(4-(((6-methoxy-2-(2-methoxyimidazo[2,1-b][1,3,4]thiadiazol-6-yl)benzofuran-4-yl)oxy)methyl)-5-methylthiazol-2-yl)morpholine)

Guidance literature:: Multi-step reaction with 2 steps

1.1: pentamethylbenzene,; boron trichloride / dichloromethane / 1.05 h / -78 °C / Inert atmosphere

2.1: lithium aluminium tetrahydride; triphenylphosphine / tetrahydrofuran / 0.08 h / 50 °C / Inert atmosphere; Sonication

2.2: 5 h / 22 °C / Inert atmosphere

With lithium aluminium tetrahydride; pentamethylbenzene,; boron trichloride; triphenylphosphine; In tetrahydrofuran; dichloromethane;