4-allyloxy-2,6-pyridinedimethyl ditosylate

Base Information

Chemical Name:4-allyloxy-2,6-pyridinedimethyl ditosylate
CAS No.:156204-46-5
Molecular Formula:C₂₄H₂₅NO₇S₂
Molecular Weight:503.597
Hs Code.:

Synonyms:4-allyloxy-2,6-pyridinedimethyl ditosylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-allyloxy-2,6-pyridinedimethyl ditosylate

Chemical Property:

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Technology Process of 4-allyloxy-2,6-pyridinedimethyl ditosylate

There total 3 articles about 4-allyloxy-2,6-pyridinedimethyl ditosylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106724-63-4
dimethyl 4-allyloxy-2,6-pyridinedicarboxylate

: 156204-46-5
4-allyloxy-2,6-pyridinedimethyl ditosylate

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄ / ethanol

2: KOH / H₂O; CH₂Cl₂

With potassium hydroxide; sodium tetrahydroborate; In ethanol; dichloromethane; water; 1: Reduction / 2: Tosylation;
DOI:10.1080/00397919908086011

Reference yield:

: 20443-03-2
4-oxo-1,4-dihydro-pyridine-2,6-dicarboxylic acid dimethyl ester

: 156204-46-5
4-allyloxy-2,6-pyridinedimethyl ditosylate

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / K₂CO₃ / dimethylformamide / 9 h / 50 °C

2: NaBH₄ / ethanol

3: KOH / H₂O; CH₂Cl₂

With potassium hydroxide; sodium tetrahydroborate; potassium carbonate; In ethanol; dichloromethane; water; N,N-dimethyl-formamide; 1: Alkylation / 2: Reduction / 3: Tosylation;
DOI:10.1080/00397919908086011