5-[(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydro-2-naphthalenyl)methyl]-2-furoic acid

Base Information

Chemical Name:5-[(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydro-2-naphthalenyl)methyl]-2-furoic acid
CAS No.:263854-27-9
Molecular Formula:C₂₁H₂₆O₃
Molecular Weight:326.436
Hs Code.:

Synonyms:5-[(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydro-2-naphthalenyl)methyl]-2-furoic acid

Suppliers and Price of 5-[(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydro-2-naphthalenyl)methyl]-2-furoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-[(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydro-2-naphthalenyl)methyl]-2-furoic acid

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Hazard Codes:

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Technology Process of 5-[(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydro-2-naphthalenyl)methyl]-2-furoic acid

There total 1 articles about 5-[(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydro-2-naphthalenyl)methyl]-2-furoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 2144-37-8
methyl 5-(chloromethyl)-2-furoate

: Methyl 5-[(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydro-2-naphthalenyl) methyl]-2-furoate

: 6683-48-3
1,1,4,4,6-pentamethyl-1,2,3,4-tetrahydronaphthalene

: 637012-34-1
5-[(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydro-2-naphthalenyl)methyl]-N'-(2,4,6-trimethoxybenzyl)-2-furohydrazide

: 263854-27-9
5-[(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydro-2-naphthalenyl)methyl]-2-furoic acid

Guidance literature:: With sodium hydroxide; aluminium trichloride; In methanol; dichloromethane; water; ethyl acetate;

Reference yield:

: 263854-27-9
5-[(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydro-2-naphthalenyl)methyl]-2-furoic acid

: 4-({[5-(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydro-naphthalen-2-ylmethyl)-furan-2-carbonyl]-amino}-methyl)-cyclohexanecarboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: SO₂Cl₂ / CH₂Cl₂ / 5 h / Heating

2: Et₃N / ethyl acetate / 20 °C

With sulfuryl dichloride; triethylamine; In dichloromethane; ethyl acetate;
DOI:10.1016/S0960-894X(02)00755-2

Reference yield:

: 263854-27-9
5-[(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydro-2-naphthalenyl)methyl]-2-furoic acid

: N-{[4-({[amino(imino)methyl]amino}methyl)cyclohexyl]methyl}-5-[(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydronaphthalen-2-yl)methyl]-2-furamide

Guidance literature:: Multi-step reaction with 3 steps

1: SO₂Cl₂ / CH₂Cl₂ / 5 h / Heating

2: Et₃N / ethyl acetate / 20 °C

3: 50 percent aq. TFA / 0.5 h / 20 °C

With sulfuryl dichloride; triethylamine; trifluoroacetic acid; In dichloromethane; ethyl acetate;
DOI:10.1016/S0960-894X(02)00755-2