(1Z,4Z,9Z,15Z)-5,10,15,20-Tetrakis-(2,4,6-trimethyl-phenyl)-porphyrin 22-oxide

Base Information

• Chemical Name: (1Z,4Z,9Z,15Z)-5,10,15,20-Tetrakis-(2,4,6-trimethyl-phenyl)-porphyrin 22-oxide
• CAS No.: 104439-49-8
• Molecular Formula: C₅₆H₅₄N₄O
• Molecular Weight: 799.071
• Mol file: 104439-49-8.mol

Synonyms:(1Z,4Z,9Z,15Z)-5,10,15,20-Tetrakis-(2,4,6-trimethyl-phenyl)-porphyrin 22-oxide

Chemical Property of (1Z,4Z,9Z,15Z)-5,10,15,20-Tetrakis-(2,4,6-trimethyl-phenyl)-porphyrin 22-oxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (1Z,4Z,9Z,15Z)-5,10,15,20-Tetrakis-(2,4,6-trimethyl-phenyl)-porphyrin 22-oxide

There total 2 articles about (1Z,4Z,9Z,15Z)-5,10,15,20-Tetrakis-(2,4,6-trimethyl-phenyl)-porphyrin 22-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

C56H52N4O(2-)*C7H4ClO2(1-)*Fe(3+) (104463-56-1) → 5,10,15,20-tetramesitylporphyrin (56396-12-4) + (1Z,4Z,9Z,15Z)-5,10,15,20-Tetrakis-(2,4,6-trimethyl-phenyl)-porphyrin 22-oxide (104439-49-8)

Guidance literature:

With hydrochloride acetic acid; at 0 ℃; for 0.0166667h;

DOI:10.1021/ja00284a059

Reference yield:

→ (1Z,4Z,9Z,15Z)-5,10,15,20-Tetrakis-(2,4,6-trimethyl-phenyl)-porphyrin 22-oxide (104439-49-8)

Guidance literature:

With hydrogenchloride; acetic acid; 3-chloro-benzenecarboperoxoic acid; Yield given. Multistep reaction; 1.) toluene, 0 deg C, 2.) toluene, 0 deg C;

DOI:10.1021/ja00233a021

upstream raw materials:

C₅₆H₅₂N₄O^(2-)*C₇H₄ClO₂^(1-)*Fe⁽³⁺⁾