3,5-difluoro-N-methyl-benzamidoxime

Base Information

• Chemical Name: 3,5-difluoro-N-methyl-benzamidoxime
• CAS No.: 908259-44-9
• Molecular Formula: C₈H₈F₂N₂O
• Molecular Weight: 186.161
• Mol file: 908259-44-9.mol

Synonyms:3,5-difluoro-N-methyl-benzamidoxime

Chemical Property of 3,5-difluoro-N-methyl-benzamidoxime

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,5-difluoro-N-methyl-benzamidoxime

There total 2 articles about 3,5-difluoro-N-methyl-benzamidoxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

3,5-difluorobenzonitrile (64248-63-1) + N-methoxylamine hydrochloride (593-56-6) → 3,5-difluoro-N-methyl-benzamidoxime (908259-44-9)

Guidance literature:

With ethylenediaminetetraacetic acid; mercaptoacetic acid; triethylamine; In methanol; water; at 25 - 65 ℃; Product distribution / selectivity;

Reference yield:

3,5-difluoro-N-methyl-benzamidoxime hydrochloride → 3,5-difluoro-N-methyl-benzamidoxime (908259-44-9)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 20 ℃; for 5h; Product distribution / selectivity;

Reference yield:

3,5-difluoro-N-methyl-benzamidoxime (908259-44-9) → 3,5-difluoro-N-methyl-benzamidoxime hydrochloride

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; Isopropyl acetate; at 10 ℃; for 0.333333h;

upstream raw materials:

3,5-difluorobenzonitrile

N-methoxylamine hydrochloride