1,6-bis-O-p-(2-methoxyethyl)phenyl-3,4-O-methoxymethylene-2,5-O-methylene-D-mannitol

Base Information

Chemical Name:1,6-bis-O-p-(2-methoxyethyl)phenyl-3,4-O-methoxymethylene-2,5-O-methylene-D-mannitol
CAS No.:114218-32-5
Molecular Formula:C₂₇H₃₆O₉
Molecular Weight:504.577
Hs Code.:

Synonyms:1,6-bis-O-p-(2-methoxyethyl)phenyl-3,4-O-methoxymethylene-2,5-O-methylene-D-mannitol

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Chemical Property of 1,6-bis-O-p-(2-methoxyethyl)phenyl-3,4-O-methoxymethylene-2,5-O-methylene-D-mannitol

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Technology Process of 1,6-bis-O-p-(2-methoxyethyl)phenyl-3,4-O-methoxymethylene-2,5-O-methylene-D-mannitol

There total 3 articles about 1,6-bis-O-p-(2-methoxyethyl)phenyl-3,4-O-methoxymethylene-2,5-O-methylene-D-mannitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 56718-71-9
4-(2-methoxyethyl)phenol

: 2,5-O-methylene-3,4-O-methoxymethylene-1,6-di-O-p-toluenesulfonyl-D-mannitol

: 114218-32-5
1,6-bis-O-p-(2-methoxyethyl)phenyl-3,4-O-methoxymethylene-2,5-O-methylene-D-mannitol

Guidance literature:: With potassium hydroxide; In acetonitrile; for 72h; Heating;

Reference yield:

: 2,5-O-methylene-D-mannitol

: 114218-32-5
1,6-bis-O-p-(2-methoxyethyl)phenyl-3,4-O-methoxymethylene-2,5-O-methylene-D-mannitol

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / pyridine / Ambient temperature

2: 100 percent / p-toluenesulfonic acid / Ambient temperature

3: 91 percent / aq. potassium hydroxide / acetonitrile / 72 h / Heating

With pyridine; potassium hydroxide; toluene-4-sulfonic acid; In acetonitrile;

Reference yield:

: 2,5-O-methylene-1,6-di-O-p-toluenesulfonyl-D-mannitol

: 114218-32-5
1,6-bis-O-p-(2-methoxyethyl)phenyl-3,4-O-methoxymethylene-2,5-O-methylene-D-mannitol

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / p-toluenesulfonic acid / Ambient temperature

2: 91 percent / aq. potassium hydroxide / acetonitrile / 72 h / Heating

With potassium hydroxide; toluene-4-sulfonic acid; In acetonitrile;