methyl 1-(4-((3-(azido(phenyl)methyl)phenoxy)methyl)-phenyl)cyclopropanecarboxylate

Base Information

Chemical Name:methyl 1-(4-((3-(azido(phenyl)methyl)phenoxy)methyl)-phenyl)cyclopropanecarboxylate
CAS No.:1416069-76-5
Molecular Formula:C₂₅H₂₃N₃O₃
Molecular Weight:413.476
Hs Code.:

Synonyms:methyl 1-(4-((3-(azido(phenyl)methyl)phenoxy)methyl)-phenyl)cyclopropanecarboxylate

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Chemical Property of methyl 1-(4-((3-(azido(phenyl)methyl)phenoxy)methyl)-phenyl)cyclopropanecarboxylate

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Technology Process of methyl 1-(4-((3-(azido(phenyl)methyl)phenoxy)methyl)-phenyl)cyclopropanecarboxylate

There total 5 articles about methyl 1-(4-((3-(azido(phenyl)methyl)phenoxy)methyl)-phenyl)cyclopropanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1416069-75-4
methyl 1-(4-((3-(hydroxy(phenyl)methyl)phenoxy)-methyl)phenyl)cyclopropanecarboxylate

: 1416069-76-5
methyl 1-(4-((3-(azido(phenyl)methyl)phenoxy)methyl)-phenyl)cyclopropanecarboxylate

Guidance literature:: With diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In toluene; at 100 ℃; for 3h; Inert atmosphere;

Reference yield:

: 83846-66-6
1-(4-methylphenyl)cyclopropanecarboxylic acid

: 1416069-76-5
methyl 1-(4-((3-(azido(phenyl)methyl)phenoxy)methyl)-phenyl)cyclopropanecarboxylate

Guidance literature:: Multi-step reaction with 5 steps

1: toluene-4-sulfonic acid / 16 h / 75 °C

2: N-Bromosuccinimide / dibenzoyl peroxide / acetonitrile / 2.67 h / 80 °C

3: potassium carbonate / N,N-dimethyl-formamide / 16 h / 60 °C

4: sodium tetrahydroborate; methanol / 2.17 h / 0 - 20 °C / Inert atmosphere

5: diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 3 h / 100 °C / Inert atmosphere

With methanol; sodium tetrahydroborate; N-Bromosuccinimide; diphenyl phosphoryl azide; potassium carbonate; toluene-4-sulfonic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; dibenzoyl peroxide; In N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 959632-00-9
methyl 1-(p-tolyl)cyclopropanecarboxylate

: 1416069-76-5
methyl 1-(4-((3-(azido(phenyl)methyl)phenoxy)methyl)-phenyl)cyclopropanecarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: N-Bromosuccinimide / dibenzoyl peroxide / acetonitrile / 2.67 h / 80 °C

2: potassium carbonate / N,N-dimethyl-formamide / 16 h / 60 °C

3: sodium tetrahydroborate; methanol / 2.17 h / 0 - 20 °C / Inert atmosphere

4: diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 3 h / 100 °C / Inert atmosphere

With methanol; sodium tetrahydroborate; N-Bromosuccinimide; diphenyl phosphoryl azide; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; dibenzoyl peroxide; In N,N-dimethyl-formamide; toluene; acetonitrile;