1-(4-((3-(azido(phenyl)methyl)phenoxy)methyl)phenyl)-cyclopropanecarboxylic acid

Base Information

Chemical Name:1-(4-((3-(azido(phenyl)methyl)phenoxy)methyl)phenyl)-cyclopropanecarboxylic acid
CAS No.:1416069-77-6
Molecular Formula:C₂₄H₂₁N₃O₃
Molecular Weight:399.449
Hs Code.:

Synonyms:1-(4-((3-(azido(phenyl)methyl)phenoxy)methyl)phenyl)-cyclopropanecarboxylic acid

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Chemical Property of 1-(4-((3-(azido(phenyl)methyl)phenoxy)methyl)phenyl)-cyclopropanecarboxylic acid

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Technology Process of 1-(4-((3-(azido(phenyl)methyl)phenoxy)methyl)phenyl)-cyclopropanecarboxylic acid

There total 6 articles about 1-(4-((3-(azido(phenyl)methyl)phenoxy)methyl)phenyl)-cyclopropanecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1416069-76-5
methyl 1-(4-((3-(azido(phenyl)methyl)phenoxy)methyl)-phenyl)cyclopropanecarboxylate

: 1416069-77-6
1-(4-((3-(azido(phenyl)methyl)phenoxy)methyl)phenyl)-cyclopropanecarboxylic acid

Guidance literature:: methyl 1-(4-((3-(azido(phenyl)methyl)phenoxy)methyl)-phenyl)cyclopropanecarboxylate; With water; sodium hydroxide; In tetrahydrofuran; methanol; at 20 - 50 ℃; for 19h;

With hydrogenchloride; In tetrahydrofuran; methanol; water; pH=4;

Reference yield:

: 83846-66-6
1-(4-methylphenyl)cyclopropanecarboxylic acid

: 1416069-77-6
1-(4-((3-(azido(phenyl)methyl)phenoxy)methyl)phenyl)-cyclopropanecarboxylic acid

Guidance literature:: Multi-step reaction with 6 steps

1.1: toluene-4-sulfonic acid / 16 h / 75 °C

2.1: N-Bromosuccinimide / dibenzoyl peroxide / acetonitrile / 2.67 h / 80 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 60 °C

4.1: sodium tetrahydroborate; methanol / 2.17 h / 0 - 20 °C / Inert atmosphere

5.1: diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 3 h / 100 °C / Inert atmosphere

6.1: sodium hydroxide; water / tetrahydrofuran; methanol / 19 h / 20 - 50 °C

6.2: pH 4

With methanol; sodium tetrahydroborate; N-Bromosuccinimide; diphenyl phosphoryl azide; water; potassium carbonate; toluene-4-sulfonic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium hydroxide; dibenzoyl peroxide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 959632-00-9
methyl 1-(p-tolyl)cyclopropanecarboxylate

: 1416069-77-6
1-(4-((3-(azido(phenyl)methyl)phenoxy)methyl)phenyl)-cyclopropanecarboxylic acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-Bromosuccinimide / dibenzoyl peroxide / acetonitrile / 2.67 h / 80 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 60 °C

3.1: sodium tetrahydroborate; methanol / 2.17 h / 0 - 20 °C / Inert atmosphere

4.1: diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 3 h / 100 °C / Inert atmosphere

5.1: sodium hydroxide; water / tetrahydrofuran; methanol / 19 h / 20 - 50 °C

5.2: pH 4

With methanol; sodium tetrahydroborate; N-Bromosuccinimide; diphenyl phosphoryl azide; water; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium hydroxide; dibenzoyl peroxide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; toluene; acetonitrile;