5-tert-butyl-2-methylphenyl 4-O-benzyl-2-O-benzoyl-1-thio-α-L-rhamnopyranoside

Base Information

Chemical Name:5-tert-butyl-2-methylphenyl 4-O-benzyl-2-O-benzoyl-1-thio-α-L-rhamnopyranoside
CAS No.:1384442-64-1
Molecular Formula:C₃₁H₃₆O₅S
Molecular Weight:520.69
Hs Code.:

Synonyms:5-tert-butyl-2-methylphenyl 4-O-benzyl-2-O-benzoyl-1-thio-α-L-rhamnopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-tert-butyl-2-methylphenyl 4-O-benzyl-2-O-benzoyl-1-thio-α-L-rhamnopyranoside

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Technology Process of 5-tert-butyl-2-methylphenyl 4-O-benzyl-2-O-benzoyl-1-thio-α-L-rhamnopyranoside

There total 3 articles about 5-tert-butyl-2-methylphenyl 4-O-benzyl-2-O-benzoyl-1-thio-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1384442-63-0
2-methyl-5-tert-butylphenyl 1-thio-L-rhamnopyranoside

: 100-39-0
benzyl bromide

: 1663-61-2
triethoxymethylbenzene

: 1384443-12-2
5-tert-butyl-2-methylphenyl 4-O-benzyl-2-O-benzoyl-1-thio-β-L-rhamnopyranoside

: 1384442-64-1
5-tert-butyl-2-methylphenyl 4-O-benzyl-2-O-benzoyl-1-thio-α-L-rhamnopyranoside

Guidance literature:: 2-methyl-5-tert-butylphenyl 1-thio-L-rhamnopyranoside; triethoxymethylbenzene; With camphor-10-sulfonic acid; In acetonitrile; at 20 ℃; for 12h;

benzyl bromide; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 2h; regioselective reaction;
DOI:10.1016/j.carres.2012.01.007

Reference yield: 29.0%

: 1384442-76-5
2-methyl-5-tert-butylphenyl 2-O-acetyl-4-azido-3-O-benzyl-4,6-dideoxy-β-D-glucopyranosyl-(1->3)-2-O-benzoyl-4-O-benzyl-1-thio-α-L-rhamnopyranoside

: 1384442-64-1
5-tert-butyl-2-methylphenyl 4-O-benzyl-2-O-benzoyl-1-thio-α-L-rhamnopyranoside

: 1384442-91-4
2-methyl-5-tert-butylphenyl 4-azido-3-O-benzyl-4,6-dideoxy-β-D-glucopyranosyl-(1->3)-2-O-benzoyl-4-O-benzyl-1-thio-α-L-rhamnopyranoside

Guidance literature:: With acetyl chloride; In methanol; dichloromethane; at 20 ℃; for 4h;
DOI:10.1016/j.carres.2012.01.007

Reference yield:

: 2-methyl-5-tert-butylphenyl 2,3,4-tri-O-acetyl-1-thio-L-rhamnopyranoside

: 1384443-12-2
5-tert-butyl-2-methylphenyl 4-O-benzyl-2-O-benzoyl-1-thio-β-L-rhamnopyranoside

: 1384442-64-1
5-tert-butyl-2-methylphenyl 4-O-benzyl-2-O-benzoyl-1-thio-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium methylate / methanol / 1 h / 20 °C

2.1: camphor-10-sulfonic acid / acetonitrile / 12 h / 20 °C

2.2: 2 h / 0 - 20 °C

With camphor-10-sulfonic acid; sodium methylate; In methanol; acetonitrile;
DOI:10.1016/j.carres.2012.01.007