(2S)-({[3-(allyloxy)piperidin-1-yl]carbonyl}amino)(cyclohexyl)acetic acid

Base Information

Chemical Name:(2S)-({[3-(allyloxy)piperidin-1-yl]carbonyl}amino)(cyclohexyl)acetic acid
CAS No.:1026200-44-1
Molecular Formula:C₁₇H₂₈N₂O₄
Molecular Weight:324.42
Hs Code.:

Synonyms:(2S)-({[3-(allyloxy)piperidin-1-yl]carbonyl}amino)(cyclohexyl)acetic acid

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Chemical Property of (2S)-({[3-(allyloxy)piperidin-1-yl]carbonyl}amino)(cyclohexyl)acetic acid

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Technology Process of (2S)-({[3-(allyloxy)piperidin-1-yl]carbonyl}amino)(cyclohexyl)acetic acid

There total 5 articles about (2S)-({[3-(allyloxy)piperidin-1-yl]carbonyl}amino)(cyclohexyl)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1026200-42-9
methyl (2S)-({[3-(allyloxy)piperidin-1-yl]carbonyl}amino)(cyclohexyl)acetate

: 1026200-44-1
(2S)-({[3-(allyloxy)piperidin-1-yl]carbonyl}amino)(cyclohexyl)acetic acid

Guidance literature:: With methanol; lithium hydroxide; water; In tetrahydrofuran; at 25 ℃; for 18h;

Reference yield:

: 85275-45-2
N-tert-butoxycarbonyl-3-piperidinol

: 1026200-44-1
(2S)-({[3-(allyloxy)piperidin-1-yl]carbonyl}amino)(cyclohexyl)acetic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium tert-butylate / dimethyl sulfoxide / 0.5 h / 20 °C / Inert atmosphere

1.2: 20 h

2.1: hydrogenchloride / ethyl acetate / 3 h / 20 °C / Cooling with ice; Inert atmosphere

3.1: tetrahydrofuran / 24 h / 20 °C

4.1: lithium hydroxide; methanol / tetrahydrofuran / 18 h / 20 °C

With hydrogenchloride; methanol; potassium tert-butylate; lithium hydroxide; In tetrahydrofuran; dimethyl sulfoxide; ethyl acetate;

Reference yield:

: 14328-63-3,14328-64-4
methyl (2S)-amino(cyclohexyl)ethanoate hydrochloride

: 1026200-44-1
(2S)-({[3-(allyloxy)piperidin-1-yl]carbonyl}amino)(cyclohexyl)acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogencarbonate / dichloromethane / 1 h / Cooling with ice

2: tetrahydrofuran / 24 h / 20 °C

3: lithium hydroxide; methanol / tetrahydrofuran / 18 h / 20 °C

With methanol; sodium hydrogencarbonate; lithium hydroxide; In tetrahydrofuran; dichloromethane;