3-Bromo-2-[(E)-methoxycarbonylimino]-3-phenyl-propionic acid ethyl ester

Base Information

• Chemical Name: 3-Bromo-2-[(E)-methoxycarbonylimino]-3-phenyl-propionic acid ethyl ester
• CAS No.: 130628-88-5
• Molecular Formula: C₁₃H₁₄BrNO₄
• Molecular Weight: 328.162

Synonyms:3-Bromo-2-[(E)-methoxycarbonylimino]-3-phenyl-propionic acid ethyl ester

Chemical Property of 3-Bromo-2-[(E)-methoxycarbonylimino]-3-phenyl-propionic acid ethyl ester

Chemical Property:

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Technology Process of 3-Bromo-2-[(E)-methoxycarbonylimino]-3-phenyl-propionic acid ethyl ester

There total 1 articles about 3-Bromo-2-[(E)-methoxycarbonylimino]-3-phenyl-propionic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

(E)-2-Methoxycarbonylamino-3-phenyl-acrylic acid ethyl ester (130628-86-3) → 3-Bromo-2-[(E)-methoxycarbonylimino]-3-phenyl-propionic acid ethyl ester (130628-88-5)

Guidance literature:

With N-Bromosuccinimide; In dichloromethane; for 12h; Ambient temperature;

DOI:10.1016/S0040-4039(00)97458-6

Reference yield: 88.0%

3-Bromo-2-[(E)-methoxycarbonylimino]-3-phenyl-propionic acid ethyl ester (130628-88-5) + ethylene glycol (107-21-1) → 3-Bromo-2-(2-hydroxy-ethoxy)-2-methoxycarbonylamino-3-phenyl-propionic acid ethyl ester (130628-98-7)

Guidance literature:

DOI:10.1016/S0040-4039(00)97458-6

Reference yield: 76.0%

3-Bromo-2-[(E)-methoxycarbonylimino]-3-phenyl-propionic acid ethyl ester (130628-88-5) → (Z)-3-bromo-2-<(methoxycarbonyl)amino>-3-phenylprop-2-enoate d'ethyle + 3-bromo-2-<(methoxycarbonyl)amino>-3-phenylprop-2-enoate d'ethyle

Guidance literature:

With triethylamine; In dichloromethane; for 2h; Ambient temperature;

upstream raw materials:

(E)-2-Methoxycarbonylamino-3-phenyl-acrylic acid ethyl ester

Downstream raw materials:

5-(Bromo-phenyl-methyl)-4,5-dihydro-[1,2,3]triazole-1,5-dicarboxylic acid 5-ethyl ester 1-methyl ester

2-(Bromo-phenyl-methyl)-2-methoxycarbonylamino-but-3-enoic acid ethyl ester

3-Bromo-2-(2-hydroxy-ethoxy)-2-methoxycarbonylamino-3-phenyl-propionic acid ethyl ester

2-(Bromo-phenyl-methyl)-aziridine-1,2-dicarboxylic acid 2-ethyl ester 1-methyl ester

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