2-(4-chlorophenyl)-6-morpholino-1H-benzo[de]isoquinoline-1,3(2H)-dione

Base Information

Chemical Name:2-(4-chlorophenyl)-6-morpholino-1H-benzo[de]isoquinoline-1,3(2H)-dione
CAS No.:330446-38-3
Molecular Formula:C₂₂H₁₇ClN₂O₃
Molecular Weight:392.842
Hs Code.:

Synonyms:2-(4-chlorophenyl)-6-morpholino-1H-benzo[de]isoquinoline-1,3(2H)-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(4-chlorophenyl)-6-morpholino-1H-benzo[de]isoquinoline-1,3(2H)-dione

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Technology Process of 2-(4-chlorophenyl)-6-morpholino-1H-benzo[de]isoquinoline-1,3(2H)-dione

There total 2 articles about 2-(4-chlorophenyl)-6-morpholino-1H-benzo[de]isoquinoline-1,3(2H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: bis(4-chlorophenyl)iodonium tetrafluoroborate

: 87223-14-1
6-morpholino-1H-benzo[de]-isoquinoline-1,3(2H)-dione

: 330446-38-3
2-(4-chlorophenyl)-6-morpholino-1H-benzo[de]isoquinoline-1,3(2H)-dione

Guidance literature:: With copper(l) iodide; potassium tert-butylate; In toluene; at 100 ℃; for 2h;
DOI:10.1055/s-0033-1339448

Reference yield:

: 26018-88-2
bis(4-chlorophenyl)iodonium bromide

: 330446-38-3
2-(4-chlorophenyl)-6-morpholino-1H-benzo[de]isoquinoline-1,3(2H)-dione

Guidance literature:: Multi-step reaction with 2 steps

1: dihydrogen peroxide; tetrafluoroboric acid / water

2: potassium tert-butylate; copper(l) iodide / toluene / 2 h / 100 °C

With copper(l) iodide; tetrafluoroboric acid; potassium tert-butylate; dihydrogen peroxide; In water; toluene;
DOI:10.1055/s-0033-1339448