[TiCl₂(N(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)C(Me)CHC(Me)N(2,4,6-trimethylsilyl))]

Base Information

• Chemical Name: [TiCl₂(N(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)C(Me)CHC(Me)N(2,4,6-trimethylsilyl))]
• CAS No.: 887947-18-4
• Molecular Formula: C₄₁H₇₇Cl₂N₂Si₆Ti
• Molecular Weight: 885.375

Synonyms:[TiCl₂(N(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)C(Me)CHC(Me)N(2,4,6-trimethylsilyl))]

Chemical Property of [TiCl₂(N(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)C(Me)CHC(Me)N(2,4,6-trimethylsilyl))]

Chemical Property:

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Technology Process of [TiCl₂(N(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)C(Me)CHC(Me)N(2,4,6-trimethylsilyl))]

There total 1 articles about [TiCl₂(N(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)C(Me)CHC(Me)N(2,4,6-trimethylsilyl))] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

tetrachlorobis(tetrahydrofuran)titanium(IV) (31011-57-1,112925-19-6,112925-18-5) + [Li(N(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)C(Me)CHC(Me)N(2,4,6-trimethylphenyl))] (676321-94-1) → [TiCl2(N(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)C(Me)CHC(Me)N(2,4,6-trimethylsilyl))] (887947-18-4)

Guidance literature:

In benzene; under Ar; soln. of Li compd. in benzene added to slurry of Ti complex inbenzene; stirred for 3 h; solvent removed under reduced pressure; toluene added; filtered through Celite; filtrate dried under vac.; recrystd. from toluene at -40°C; elem. anal.;

DOI:10.1021/om0509948

Reference yield: 81.0%

1,2-bis(dimethylphosphanyl)ethane (23936-60-9) + [TiCl2(N(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)C(Me)CHC(Me)N(2,4,6-trimethylsilyl))] (887947-18-4) → TiCl(NC6H2(CH(Si(CH3)3)2)3)(NC6H2(CH3)3CCH3CHCCH3)(CH3)2PCH2CH2P(CH3)2

Guidance literature:

With KC₈; In benzene; (Ar); addn. of KC8 to a soln. of titanium complex and diphosphine in benzene, stirring for 1 d at room temp.; evapn. in vac., addn. of benzene, filtration through Celite, evapn. in vac., recrystn. (toluene, -40°C);

DOI:10.1021/ic0620844

upstream raw materials:

tetrachlorobis(tetrahydrofuran)titanium(IV)

[Li(N(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)C(Me)CHC(Me)N(2,4,6-trimethylphenyl))]

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