2-Mercapto-7,7-dimethyl-4-(4-nitro-phenyl)-5-oxo-1,4,5,6,7,8-hexahydro-quinoline-3-carbonitrile; compound with morpholine

Base Information

Chemical Name:2-Mercapto-7,7-dimethyl-4-(4-nitro-phenyl)-5-oxo-1,4,5,6,7,8-hexahydro-quinoline-3-carbonitrile; compound with morpholine
CAS No.:131270-84-3
Molecular Formula:C₄H₉NO*C₁₈H₁₇N₃O₃S
Molecular Weight:442.539
Hs Code.:

Synonyms:2-Mercapto-7,7-dimethyl-4-(4-nitro-phenyl)-5-oxo-1,4,5,6,7,8-hexahydro-quinoline-3-carbonitrile; compound with morpholine

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Chemical Property of 2-Mercapto-7,7-dimethyl-4-(4-nitro-phenyl)-5-oxo-1,4,5,6,7,8-hexahydro-quinoline-3-carbonitrile; compound with morpholine

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Technology Process of 2-Mercapto-7,7-dimethyl-4-(4-nitro-phenyl)-5-oxo-1,4,5,6,7,8-hexahydro-quinoline-3-carbonitrile; compound with morpholine

There total 5 articles about 2-Mercapto-7,7-dimethyl-4-(4-nitro-phenyl)-5-oxo-1,4,5,6,7,8-hexahydro-quinoline-3-carbonitrile; compound with morpholine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 131270-74-1
2-Cyano-3-(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-3-(4-nitro-phenyl)-thiopropionamide; compound with morpholine

: 131270-84-3
2-Mercapto-7,7-dimethyl-4-(4-nitro-phenyl)-5-oxo-1,4,5,6,7,8-hexahydro-quinoline-3-carbonitrile; compound with morpholine

Guidance literature:: In ethanol; a) reflux, 3-4 h, b) 0 deg C, 12 h;

Reference yield: 63.0%

: 110-91-8,99108-56-2
morpholine

: 131270-70-7
2-Cyano-3-(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-3-(4-nitro-phenyl)-thiopropionamide

: 131270-84-3
2-Mercapto-7,7-dimethyl-4-(4-nitro-phenyl)-5-oxo-1,4,5,6,7,8-hexahydro-quinoline-3-carbonitrile; compound with morpholine

Guidance literature:: In ethanol; a) 25 deg C, 2-3 h, b) reflux, 4-5 h, c) 0 deg C, 10-12 h;

Reference yield:

: 126-81-8
dimedone

: 131270-84-3
2-Mercapto-7,7-dimethyl-4-(4-nitro-phenyl)-5-oxo-1,4,5,6,7,8-hexahydro-quinoline-3-carbonitrile; compound with morpholine

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / ethanol / 5 h / 25 °C

2: 66 percent / ethanol / a) reflux, 3-4 h, b) 0 deg C, 12 h

In ethanol;