2-Cyano-3-(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-3-(4-nitro-phenyl)-thiopropionamide

Base Information

• Chemical Name: 2-Cyano-3-(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-3-(4-nitro-phenyl)-thiopropionamide
• CAS No.: 131270-70-7
• Molecular Formula: C₁₈H₁₉N₃O₄S
• Molecular Weight: 373.433

Synonyms:2-Cyano-3-(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-3-(4-nitro-phenyl)-thiopropionamide

Chemical Property of 2-Cyano-3-(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-3-(4-nitro-phenyl)-thiopropionamide

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Technology Process of 2-Cyano-3-(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-3-(4-nitro-phenyl)-thiopropionamide

There total 4 articles about 2-Cyano-3-(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-3-(4-nitro-phenyl)-thiopropionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

2-Cyano-3-(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-3-(4-nitro-phenyl)-thiopropionamide; compound with piperidine (131270-71-8) → 2-Cyano-3-(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-3-(4-nitro-phenyl)-thiopropionamide (131270-70-7)

Guidance literature:

With hydrogenchloride; In ethanol; at 0 ℃;

Reference yield: 88.0%

2-Cyano-3-(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-3-(4-nitro-phenyl)-thiopropionamide; compound with morpholine (131270-74-1) → 2-Cyano-3-(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-3-(4-nitro-phenyl)-thiopropionamide (131270-70-7)

Guidance literature:

With hydrogenchloride; In ethanol; at 0 ℃;

Reference yield: 88.0%

2-Cyano-3-(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-3-(4-nitro-phenyl)-thiopropionamide; compound with azepane (131270-72-9) → 2-Cyano-3-(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-3-(4-nitro-phenyl)-thiopropionamide (131270-70-7)

Guidance literature:

With hydrogenchloride; In ethanol; at 0 ℃;

upstream raw materials:

2-Cyano-3-(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-3-(4-nitro-phenyl)-thiopropionamide; compound with diethyl-amine

2-Cyano-3-(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-3-(4-nitro-phenyl)-thiopropionamide; compound with piperidine

2-Cyano-3-(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-3-(4-nitro-phenyl)-thiopropionamide; compound with morpholine

2-Cyano-3-(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-3-(4-nitro-phenyl)-thiopropionamide; compound with azepane

Downstream raw materials:

2-Mercapto-7,7-dimethyl-4-(4-nitro-phenyl)-5-oxo-1,4,5,6,7,8-hexahydro-quinoline-3-carbonitrile; compound with morpholine

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